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网站主页CAS数据库列表 1008-76-0更多图谱γ-苯基-γ-丁内酯(1008-76-0)核磁图(1HNMR)

γ-苯基-γ-丁内酯

产品名称 γ-苯基-γ-丁内酯

CAS号1008-76-0

分子式C10H10O2

分子量162.19

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  • Mass

    MS-KW-0534          
    gamma-phenyl-gamma-butyrolactone
    C10H10O2            (Mass of molecular ion:    162)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       2.1
          26.0       1.5
          27.0       7.3
          28.0      33.1
          29.0       7.7
          38.0       2.0
          39.0      10.6
          40.0       1.0
          41.0       1.4
          42.0       1.7
          50.0       8.3
          51.0      20.9
          52.0       5.1
          53.0       1.8
          55.0       4.3
          56.0      79.2
          57.0       6.2
          57.5       3.5
          58.0       5.3
          62.0       2.5
          63.0       6.6
          64.0       1.5
          65.0       5.9
          66.0       1.4
          74.0       2.8
          75.0       2.2
          76.0       2.7
          77.0      31.7
          78.0      16.3
          79.0      16.9
          80.0       1.1
          84.0       1.7
          85.0       4.4
          89.0       4.6
          90.0       1.6
          91.0      15.3
          92.0       1.8
         102.0       1.2
         103.0       3.9
         104.0       1.6
         105.0      60.0
         106.0       9.1
         107.0      90.3
         108.0       6.9
         115.0      18.3
         116.0       7.0
         117.0      33.7
         118.0      19.3
         119.0       1.9
         120.0       2.0
         133.0       3.1
         134.0       1.6
         144.0      11.2
         145.0       1.3
         161.0      16.2
         162.0     100.0
         163.0      11.7
         164.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10H10O2 0.041 g : 0.5 ml CDCl3
    gamma-phenyl-gamma-butyrolactone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.410 B 7.33 C 5.496 D *1 2.64 E *1 2.178

         Hz     ppm     Int.
    

       2959.84   7.404    141
       2958.13   7.400    193
       2956.67   7.396    128
       2953.86   7.389    163
       2952.76   7.386    339
       2950.93   7.382    382
       2950.32   7.380    366
       2949.35   7.378    361
       2947.39   7.373    218
       2945.81   7.369    158
       2944.22   7.365    706
       2943.36   7.363    717
       2942.02   7.360    199
       2938.48   7.351    132
       2937.38   7.348    193
       2936.41   7.345    310
       2935.31   7.343    458
       2931.28   7.333    960
       2928.59   7.326    469
       2925.79   7.319    220
       2925.05   7.317    263
       2923.83   7.314    424
       2922.49   7.311    288
       2920.66   7.306    105
       2204.35   5.514    161
       2198.25   5.499    186
       2196.42   5.495    199
       2190.19   5.479    199
       1075.69   2.691     61
       1069.83   2.677    109
       1066.78   2.669    123
       1064.34   2.663    171
       1061.04   2.655    328
       1060.43   2.653    239
       1058.84   2.649    237
       1057.38   2.645   1000
       1056.65   2.644    867
       1056.16   2.642    828
       1053.11   2.635    356
       1051.88   2.632    614
       1051.40   2.630    712
       1049.81   2.626    191
       1048.59   2.623    183
       1046.15   2.617    238
       1045.66   2.616    261
       1044.32   2.613    223
       1043.71   2.611    202
       1039.68   2.601     46
        895.27   2.240     47
        884.89   2.214    161
        883.55   2.211     82
        882.21   2.207     62
        878.79   2.199     99
        876.35   2.193    138
        875.01   2.189     89
        872.32   2.182     99
        871.59   2.181    225
        870.49   2.178    156
        868.17   2.172    150
        867.19   2.170    198
        862.19   2.157    136
        860.48   2.153     49
        859.01   2.149    131
        858.28   2.147     63
        854.38   2.138     65
        851.45   2.130     22
        845.95   2.117     51
    

in CDCl3



KBr disk