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MassMS-NW-9731 N,N'-diethyltrimethylenediamine C7H18N2 (Mass of molecular ion: 130)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.0 18.0 3.2 27.0 4.7 28.0 13.2 29.0 8.8 30.0 58.0 31.0 1.0 39.0 1.4 41.0 6.7 42.0 8.6 43.0 4.6 44.0 25.8 45.0 12.9 46.0 1.3 50.0 6.3 54.0 1.1 56.0 18.5 57.0 7.0 58.0 100.0 59.0 4.9 68.0 1.2 70.0 91.2 71.0 6.7 72.0 19.3 73.0 1.5 84.0 8.7 85.0 72.6 86.0 6.3 87.0 6.7 130.0 1.2 131.0 2.2 141.0 3.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H18 N2 0.05 ml : 0.5 ml CDCl3 N,N'-diethyltrimethylenediamine 
Assign. Shift(ppm)
A 2.676 B 2.645 C 1.691 D 1.46 E 1.105
Hz ppm Int.1076.90 2.695 355 1069.82 2.677 594 1067.87 2.673 289 1062.87 2.660 404 1060.67 2.654 642 1057.01 2.645 40 1053.47 2.636 639 1050.17 2.628 36 1046.39 2.619 262 689.82 1.727 56 682.74 1.709 188 675.66 1.691 244 668.58 1.673 171 661.74 1.656 53 583.01 1.459 145 448.97 1.124 610 441.77 1.106 1000 434.69 1.088 669
in CDCl3
liquid film
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