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MassMS-NW-5644 2,6-dimethylanisole C9H12O (Mass of molecular ion: 136)
Source Temperature: 280 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.9 27.0 5.2 38.0 1.3 39.0 9.5 40.0 1.3 41.0 3.8 43.0 1.4 50.0 2.8 51.0 7.6 52.0 3.2 53.0 5.3 62.0 1.5 63.0 4.1 64.0 1.1 65.0 7.8 66.0 1.1 77.0 34.5 78.0 9.2 79.0 4.8 89.0 1.2 91.0 33.4 92.0 4.2 93.0 9.4 103.0 6.4 104.0 5.3 105.0 13.1 106.0 2.4 107.0 1.1 121.0 84.6 122.0 9.4 135.0 3.8 136.0 100.0 137.0 10.1
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C9 H12 O 0.04 ml : 0.5 ml CDCl3 2,6-dimethylanisole 
Assign. Shift(ppm)
A 7.00 B 6.90 C 3.707 D 2.277
Hz ppm Int.628.31 7.016 25 624.38 6.972 125 623.94 6.967 131 622.00 6.946 179 618.06 6.902 28 332.06 3.708 1000 330.19 3.687 21 203.94 2.278 725
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1H NMR 399.65 MHz C9 H12 O 0.05 ml : 0.5 ml CDCl3 2,6-dimethylanisole Assign. Shift(ppm)
A 6.975 B 6.889 C 3.684 D 2.269 90MHZ. : HSP-03-275
Hz ppm Int.2792.48 6.988 137 2791.75 6.986 137 2791.14 6.984 104 2785.77 6.971 158 2785.16 6.969 224 2784.55 6.968 229 2783.94 6.966 173 2759.52 6.905 122 2752.93 6.889 88 2751.34 6.885 83 2744.63 6.868 56 1472.41 3.685 1000 907.23 2.271 815 906.49 2.269 854
liquid film
4880 A,200 M,liquid
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