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MassMS-IW-5793 1,1'-(oxybis(o-phenylene))dimethanol C14H14O3 (Mass of molecular ion: 230)
Source Temperature: 160 °C Sample Temperature: 130 °C Direct, 75 eV
17.0 2.0 18.0 10.3 27.0 3.9 28.0 2.4 29.0 2.1 31.0 3.4 38.0 1.1 39.0 10.6 40.0 1.6 41.0 2.7 50.0 4.4 51.0 18.5 52.0 5.1 53.0 5.1 55.0 5.6 62.0 1.4 63.0 6.6 64.0 4.0 65.0 10.5 66.0 2.1 74.0 1.4 75.0 1.9 76.0 8.5 76.5 1.2 77.0 42.8 78.0 20.0 79.0 10.8 81.0 1.0 82.0 2.1 82.5 1.7 83.0 1.3 84.0 1.1 89.0 6.8 90.0 11.7 90.5 2.0 91.0 47.9 91.5 1.0 92.0 12.9 93.0 4.4 94.0 2.6 95.0 2.7 97.0 5.4 97.5 1.2 104.0 2.9 105.0 14.9 106.0 16.6 107.0 11.5 108.0 1.6 114.0 1.2 115.0 7.6 116.0 1.4 118.0 23.4 119.0 7.8 120.0 48.5 121.0 32.0 122.0 5.8 123.0 1.5 127.0 3.3 128.0 4.7 129.0 3.3 131.0 1.6 135.0 1.4 139.0 3.0 141.0 5.5 142.0 1.0 144.0 1.8 151.0 2.3 152.0 11.1 153.0 9.9 154.0 3.5 155.0 11.8 156.0 2.0 165.0 22.7 166.0 8.9 167.0 8.2 168.0 6.3 169.0 6.7 170.0 1.3 171.0 3.6 177.0 3.6 178.0 1.3 181.0 66.3 182.0 13.2 183.0 28.2 184.0 7.2 185.0 1.0 193.0 3.3 194.0 44.3 195.0 70.9 196.0 16.2 197.0 25.6 198.0 3.9 199.0 2.4 209.0 1.7 210.0 3.8 211.0 45.7 212.0 100.0 213.0 15.3 214.0 2.4 230.0 22.5 231.0 3.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H14 O3 0.038 g : 0.5 ml CDCl3 1,1'-(oxybis(o-phenylene))dimethanol 
Assign. Shift(ppm)
A 7.333 B 7.215 C 7.072 D 6.792 E 4.583 F 3.64
Hz ppm Int.2937.87 7.352 520 2936.28 7.348 534 2930.42 7.333 597 2928.83 7.329 596 2892.94 7.239 301 2891.24 7.235 289 2885.25 7.220 561 2883.67 7.216 518 2880.62 7.208 52 2877.44 7.200 433 2875.61 7.196 382 2833.62 7.091 466 2832.52 7.088 468 2826.17 7.072 757 2825.07 7.069 738 2818.73 7.053 335 2817.63 7.051 317 2718.75 6.803 751 2717.77 6.801 720 2710.69 6.783 696 2709.72 6.781 653 1834.11 4.590 963 1829.10 4.577 1000 1461.67 3.658 216 1456.42 3.645 497 1451.05 3.631 196
in CDCl3
KBr disc
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