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网站主页CAS数据库列表 1002-28-4更多图谱3-已炔-1-醇(1002-28-4)核磁图(13CNMR)

3-已炔-1-醇

产品名称 3-已炔-1-醇

CAS号1002-28-4

分子式C6H10O

分子量98.14

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  • Mass

    MS-NW-3225          
    3-hexyn-1-ol
    C6H10O              (Mass of molecular ion:     98)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.4
          18.0       1.3
          26.0       2.1
          27.0      12.7
          28.0       2.2
          29.0       6.8
          31.0      27.6
          37.0       2.0
          38.0       3.8
          39.0      30.0
          40.0      17.3
          41.0      50.3
          42.0      12.0
          43.0       8.0
          44.0       1.8
          50.0       5.2
          51.0       9.0
          52.0       6.8
          53.0      45.3
          54.0       3.5
          55.0       7.8
          56.0       2.2
          57.0       2.6
          61.0       1.3
          62.0       2.4
          63.0       4.0
          65.0      14.0
          66.0       6.3
          67.0      63.1
          68.0     100.0
          69.0       8.7
          70.0       1.8
          77.0       5.5
          79.0      13.6
          80.0       6.0
          81.0       1.2
          83.0       8.6
          97.0       1.1
          98.0      13.2
          99.0       1.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H10 O 0.04 ml : 0.5 ml CDCl3
    3-hexyn-1-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.666 B 2.46 C 2.42 D 2.18 E 1.128 J(C,D)=2.3HZ. J(A,B)=0.3HZ.

         Hz     ppm     Int.
    

        335.25   3.744    228
        328.56   3.669    646
        322.31   3.599    288
        225.00   2.513     87
        222.69   2.487    152
        220.50   2.463    254
        220.13   2.458    259
        218.75   2.443    194
        216.38   2.417    283
        214.06   2.391    174
        212.75   2.376     47
        211.94   2.367     48
        209.94   2.345    106
        207.69   2.320    119
        206.88   2.310     48
        206.00   2.301     39
        201.63   2.252     49
        200.88   2.243    134
        198.56   2.218    134
        196.50   2.195     59
        195.81   2.187     48
        194.31   2.170     60
        193.63   2.163     91
        193.25   2.158     88
        192.06   2.145     87
        191.06   2.134    173
        189.63   2.118     46
        188.69   2.107    104
        186.81   2.086     39
        185.81   2.075     39
        184.38   2.059     55
        183.63   2.051     61
        181.88   2.031     32
        181.31   2.025     31
        108.38   1.211    217
        107.88   1.205    364
        100.75   1.125   1000
        100.13   1.119    477
         93.00   1.039    254
         92.38   1.032    150
    

in CDCl3



liquid film