-
MS-NW-4692 4-vinylpyridine C7H7N (Mass of molecular ion: 105)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 1.3 26.0 4.1 27.0 4.2 28.0 6.7 37.0 2.1 38.0 2.9 39.0 10.7 40.0 1.0 41.0 1.2 49.0 1.9 50.0 14.3 51.0 25.4 52.0 27.3 52.5 1.3 53.0 2.8 54.0 1.8 61.0 1.2 62.0 1.6 63.0 4.5 64.0 1.3 65.0 8.9 66.0 1.5 74.0 2.1 75.0 2.4 76.0 4.2 77.0 15.5 78.0 39.7 79.0 12.6 92.0 1.4 93.0 1.8 104.0 40.5 105.0 100.0 106.0 9.5 107.0 2.1 119.0 1.4
parameter in CCl4
-
1H NMR 300 MHz C7 H7 N 10 wt% in CCl4 4-vinylpyridine Parameter ppm Hz
D(A) 8.470 D(B) 7.150 D(C) 6.574 D(D) 5.371 D(E) 5.871 J(A,A') 0.0 J(A,B) 5.10 J(A,B') 0.92 J(A,C) 0.35 J(A,D) 0.0 J(A,E) 0.0 J(A',B) 0.92 J(A',B') 5.10 J(A',C) 0.35 J(A',D) 0.0 J(A',E) 0.0 J(B,B') 1.92 J(B,C) -0.52 J(B,D) 0.15 J(B,E) 0.0 J(B',C) -0.52 J(B',D) 0.15 J(B',E) 0.0 J(C,D) 10.86 J(C,E) 17.57 J(D,E) 0.08 ROWBOTHAM,J.B. & SCHAEFER,T. CAN.J.CHEM. 52, 136 (1974)
Hz ppm Int.
2544.10 8.480 970 2542.40 8.475 604 2539.67 8.466 621 2537.97 8.460 1000 2148.12 7.160 858 2146.51 7.155 537 2143.48 7.145 525 2141.90 7.140 829 1986.89 6.623 243 1976.00 6.587 260 1969.27 6.564 287 1958.47 6.528 302 1769.73 5.899 978 1752.17 5.841 828 1616.66 5.389 872 1605.82 5.353 811
更多供应商