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MassMS-NW-4719 (p-nitrophenyl)hydrazine C6H7N3O2 (Mass of molecular ion: 153)
Source Temperature: 170 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 3.2 27.0 1.8 28.0 5.2 29.0 2.5 30.0 6.0 31.0 2.8 37.0 1.9 38.0 4.4 39.0 10.0 40.0 1.5 41.0 3.9 43.0 1.0 50.0 8.8 51.0 9.7 52.0 9.3 53.0 10.9 54.0 2.7 61.0 1.4 62.0 3.2 63.0 22.7 64.0 13.7 65.0 7.3 66.0 1.6 67.0 1.8 74.0 3.0 75.0 3.1 76.0 5.3 77.0 8.8 78.0 4.9 79.0 3.9 80.0 20.2 81.0 1.7 90.0 32.1 91.0 12.5 92.0 3.2 93.0 1.4 105.0 2.4 106.0 5.4 107.0 16.5 108.0 2.1 122.0 1.4 123.0 18.4 124.0 1.5 137.0 1.5 138.0 1.6 151.0 1.4 153.0 100.0 154.0 7.7
400 MHz in DMSO-d6
90 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H7 N3 O2 0.041 g : 0.5 ml DMSO-d6 (p-nitrophenyl)hydrazine 
Assign. Shift(ppm)
A 8.41 B 8.011 C 6.815 D 4.51
Hz ppm Int.3360.47 8.409 458 3352.78 8.390 29 3206.54 8.024 802 3197.14 8.000 842 2736.21 6.847 25 2728.03 6.827 449 2719.12 6.804 440 2710.08 6.782 28 2709.23 6.780 24 1812.74 4.536 25 1811.89 4.534 25 1802.37 4.510 1000 1793.21 4.487 43
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1H NMR 89.56 MHz C6 H7 N3 O2 0.044 g : 0.5 ml DMSO-d6 (p-nitrophenyl)hydrazine Assign. Shift(ppm)
A 8.35 B 8.00 C 6.81 D 4.48
Hz ppm Int.747.88 8.351 227 724.38 8.089 68 721.25 8.054 741 719.25 8.031 201 717.31 8.010 45 716.25 7.998 29 713.94 7.972 204 711.94 7.950 913 708.81 7.915 99 617.38 6.894 107 614.25 6.859 1000 612.13 6.835 254 609.63 6.807 30 608.69 6.797 22 606.94 6.777 217 604.88 6.754 821 601.75 6.719 92 400.75 4.475 596
in DMSO-d6
KBr disc
nujol mull
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