(1S)-(-)-6,6-DIMETHYLBICYCLO(3.1.1)HEPT-2-ENE-2-ETHANOL
Product Name (1S)-(-)-6,6-DIMETHYLBICYCLO(3.1.1)HEPT-2-ENE-2-ETHANOL
MFC11H18O
MW166.26002
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MassMS-NW-8509 (1S)-(-)-6,6-dimethylbicyclo(3.1.1)hept-2-ene-2-ethanol C11H18O (Mass of molecular ion: 166)
Source Temperature: 250 °C Sample Temperature: 140 °C Reservoir, 75 eV
27.0 10.6 28.0 1.8 29.0 7.3 31.0 4.7 39.0 12.3 40.0 2.1 41.0 24.6 42.0 1.4 43.0 13.1 50.0 1.0 51.0 4.1 52.0 2.0 53.0 8.7 54.0 1.1 55.0 9.7 56.0 1.0 57.0 1.1 63.0 1.4 65.0 5.7 66.0 3.0 67.0 7.2 68.0 2.8 69.0 5.7 77.0 16.5 78.0 5.0 79.0 26.1 80.0 4.0 81.0 4.7 82.0 1.2 83.0 1.0 91.0 24.7 92.0 18.1 93.0 20.9 94.0 2.8 95.0 2.1 103.0 4.3 104.0 1.5 105.0 100.0 106.0 10.2 107.0 7.7 115.0 1.0 117.0 1.7 119.0 4.0 120.0 1.7 121.0 6.2 122.0 10.2 123.0 1.8 133.0 7.9 135.0 5.2 148.0 1.0 151.0 2.8 166.0 3.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H18 O 0.04 ml : 0.5 ml CDCl3 (1S)-(-)-6,6-dimethylbicyclo(3.1.1)hept-2-ene-2-ethanol 
Assign. Shift(ppm)
A 5.335 B 3.604 C 2.382 D *1 2.27 E 2.23 F *1 2.22 G 2.105 J 2.040 K 1.88 L *2 1.280 M 1.148 N *2 0.846 ASSIGNED BY C-H AND H-H COSY
Hz ppm Int.2135.99 5.345 51 2134.52 5.341 82 2133.06 5.338 111 2131.71 5.334 131 2130.25 5.331 117 2128.78 5.327 74 1451.90 3.633 40 1447.75 3.623 124 1445.43 3.617 153 1441.41 3.607 245 1439.21 3.602 252 1434.94 3.591 132 1432.86 3.586 127 962.28 2.408 73 956.54 2.394 124 953.74 2.387 82 951.05 2.380 90 948.00 2.373 123 942.50 2.359 85 906.86 2.270 80 905.27 2.266 98 902.47 2.259 70 902.22 2.258 70 899.90 2.252 94 898.68 2.249 139 897.22 2.246 145 896.00 2.242 113 893.55 2.236 187 892.21 2.233 271 890.99 2.230 301 887.21 2.220 83 885.62 2.216 122 884.40 2.213 114 882.93 2.210 39 874.15 2.188 33 847.90 2.122 34 846.68 2.119 36 844.97 2.115 58 843.63 2.111 58 842.04 2.107 69 840.82 2.104 70 839.23 2.100 63 837.89 2.097 52 836.18 2.093 42 834.96 2.090 41 820.80 2.054 86 819.34 2.051 89 815.31 2.041 114 813.84 2.037 115 809.69 2.026 52 808.23 2.023 50 749.27 1.875 39 511.72 1.281 944 463.26 1.160 226 454.59 1.138 217 338.13 0.847 1000
in CDCl3
liquid film
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