TRANS-3-(4-PYRIDYL)ACRYLALDEHYDEOXALATE

Mass

MS-IW-4853          
trans-3-(4-pyridyl)acrylaldehyde oxalate
C8H7NO C2H2O4       (Mass of molecular ion:    133)

   Source Temperature: 140 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      17.0       1.9
      18.0       9.4
      26.0       1.8
      27.0       2.4
      28.0      17.0
      29.0       4.1
      37.0       1.2
      38.0       1.8
      39.0       3.9
      44.0      34.8
      45.0      12.2
      46.0       8.4
      49.0       1.3
      50.0      11.9
      51.0      28.2
      52.0      11.8
      52.5       2.0
      53.0       1.7
      54.0       2.6
      55.0       1.5
      62.0       1.8
      63.0       3.6
      64.0       1.1
      65.0       2.8
      66.0       1.7
      74.0       2.7
      75.0       3.2
      76.0       4.4
      77.0      17.3
      78.0      29.7
      79.0      21.7
      80.0       2.1
      89.0       1.0
      90.0       1.3
     102.0       1.6
     103.0       1.7
     104.0      41.9
     105.0      19.7
     106.0       2.3
     117.0       2.3
     130.0       1.7
     132.0      31.4
     133.0     100.0
     134.0       9.2
     135.0       1.1
     159.0       1.5

Assign. Shift(ppm) A 13.1 B 9.770 C 8.705 D 7.726 E 7.71 F 7.042

     Hz     ppm     Int.

   5222.86  13.069     87
   3911.27   9.787     37
   3908.50   9.780    804
   3901.02   9.762    837
   3481.77   8.713    372
   3476.64   8.700    388
   3095.85   7.747    448
   3091.58   7.736     45
   3090.09   7.732     47
   3084.32   7.718    716
   3082.82   7.714    519
   3079.83   7.707   1000
   3078.33   7.703    815
   2825.76   7.071    402
   2818.28   7.052    406
   2814.65   7.043     22
   2813.79   7.041     21
   2812.30   7.037     27
   2809.73   7.031    355
   2802.25   7.012    343