5,6,11,12-TETRAHYDRODIBENZ B F AZOCINE HYDROCHLORIDE

Mass

MS-NW-6749          
5,6,11,12-tetrahydrodibenz(b,f)azocine hydrochloride
C15H15N HCl         (Mass of molecular ion:    209)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       1.6
      27.0       1.9
      28.0       1.2
      35.0       2.5
      36.0      17.3
      38.0       5.7
      39.0       6.1
      41.0       1.2
      50.0       2.9
      51.0       6.8
      52.0       3.3
      53.0       1.2
      62.0       1.6
      63.0       5.3
      64.0       1.7
      65.0       6.8
      66.0       1.2
      74.0       1.2
      75.0       1.7
      76.0       2.8
      77.0      10.0
      78.0      12.4
      79.0       1.7
      83.5       1.6
      88.0       1.1
      89.0       6.2
      90.0       4.4
      90.5       2.2
      91.0      13.4
      92.0       2.1
      93.0       5.4
      95.5       1.2
      96.5       3.9
      97.0       1.5
     102.0       3.3
     102.5       1.8
     103.0      12.0
     103.5       4.2
     104.0      12.7
     104.5       2.8
     105.0       2.3
     106.0       2.8
     115.0       7.5
     116.0       4.9
     117.0      13.7
     118.0      59.1
     119.0       5.7
     127.0       1.0
     128.0       1.9
     130.0       3.4
     132.0       1.2
     139.0       1.0
     151.0       1.3
     152.0       3.0
     153.0       1.2
     165.0       6.0
     166.0       2.6
     167.0       3.1
     168.0       1.1
     176.0       1.5
     177.0       2.4
     178.0       7.1
     179.0       4.2
     180.0       7.2
     181.0       2.3
     189.0       2.0
     190.0       1.6
     191.0       6.6
     192.0       9.7
     193.0      18.2
     194.0      58.8
     195.0       9.3
     204.0       2.4
     205.0       1.3
     206.0       5.1
     207.0       4.0
     208.0      37.0
     209.0     100.0
     210.0      16.2
     211.0       1.4

Assign. Shift(ppm) A 11.8 B 7.63 C 7.30 to 6.88 D 4.807 E 3.40

     Hz     ppm     Int.

   1055.55  11.786     62
    688.46   7.688     77
    685.99   7.660     61
    683.59   7.633    106
    682.74   7.624     97
    679.66   7.589    124
    645.74   7.211     36
    642.75   7.177     34
    639.76   7.144    313
    635.57   7.097    280
    634.12   7.081    688
    633.44   7.073    710
    631.98   7.057    762
    630.19   7.037    387
    628.22   7.015    350
    624.38   6.972    134
    623.52   6.963     95
    620.10   6.924     41
    618.65   6.908     51
    618.31   6.904     50
    435.79   4.866     88
    435.02   4.858     92
    434.17   4.848     88
    433.74   4.844     89
    433.23   4.838     95
    432.63   4.831    112
    430.66   4.809    166
    426.73   4.765     93
    426.31   4.761     97
    425.71   4.754     97
    309.41   3.455     44
    309.07   3.451     45
    308.64   3.447     47
    304.88   3.405   1000
    296.68   3.313     34