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S-Benzoyl-N-(o-hydroxybenzylidene)thiohydroxylamine

Product Name S-Benzoyl-N-(o-hydroxybenzylidene)thiohydroxylamine

CAS

MFC14H11NO2S

MW257.30764

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  • cb02232829_ms_1
    Mass

    MS-NW-7306          
    S-benzoyl-N-(o-hydroxybenzylidene)thiohydroxylamine
    C14H11NO2S          (Mass of molecular ion:    257)
    

       Source Temperature: 160 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          17.0       1.5
          18.0       5.4
          27.0       3.3
          28.0       3.2
          37.0       1.7
          38.0       3.5
          39.0      12.5
          45.0       1.8
          50.0       9.2
          51.0      24.6
          52.0       3.1
          53.0       2.2
          62.0       1.7
          63.0       5.7
          64.0       4.3
          65.0       6.5
          66.0       2.2
          69.0       1.1
          74.0       2.4
          75.0       2.6
          76.0       3.1
          77.0      57.1
          78.0       4.6
          81.0       1.1
          90.0       2.1
          91.0       5.0
          92.0       1.4
          93.0       2.2
          97.0       1.7
         102.0       1.2
         105.0     100.0
         106.0       7.9
         119.0       2.2
         120.0       1.0
         121.0       1.6
         136.0       3.9
         152.0       1.1
         225.0       1.7
         257.0       4.1
    

400 MHz in CDCl3

  • cb02232829_1hnmr_0

    1H NMR 399.65 MHz
    C14 H11 N O2 S 0.015 g : 0.5 ml CDCl3
    S-benzoyl-N-(o-hydroxybenzylidene)thiohydroxylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.09 B 8.815 C 7.926 D 7.636 E 7.513 F 7.370 G 7.26 J 7.061 K 6.920

         Hz     ppm     Int.
    

       4831.20  12.089    387
       3521.93   8.813    390
       3173.18   7.940     37
       3171.53   7.936    213
       3170.98   7.935    153
       3170.25   7.933    275
       3169.51   7.931    109
       3169.15   7.930     99
       3168.60   7.929     85
       3165.12   7.920     76
       3163.10   7.915    291
       3161.82   7.912    261
       3160.90   7.910     64
       3060.53   7.659     38
       3059.25   7.655     73
       3057.96   7.652     42
       3053.75   7.642     48
       3052.47   7.638     78
       3051.92   7.637    139
       3050.09   7.632     55
       3045.69   7.621     71
       3044.41   7.618    124
       3043.13   7.615     64
       3009.79   7.532     49
       3008.51   7.528    159
       3008.14   7.527    195
       3007.59   7.526    109
       3006.49   7.523     84
       3003.01   7.515     33
       3001.73   7.511    123
       3001.18   7.510    147
       3000.63   7.509    212
       3000.08   7.507    250
       2998.99   7.505     77
       2994.59   7.494     53
       2993.31   7.490     77
       2992.76   7.489    134
       2992.21   7.488     95
       2991.11   7.485     33
       2953.01   7.389     53
       2951.54   7.386     56
       2945.68   7.371     64
       2944.58   7.368     94
       2943.30   7.365     73
       2937.44   7.351     63
       2935.98   7.347     67
       2902.27   7.263    134
       2900.99   7.259   1000
       2894.76   7.244    125
       2892.93   7.239    118
       2825.71   7.071    129
       2825.16   7.070    126
       2824.61   7.068    136
       2817.28   7.050    114
       2816.73   7.048    109
       2816.18   7.047    116
       2772.22   6.937     99
       2771.13   6.934    102
       2765.08   6.919    122
       2764.72   6.918    119
       2763.98   6.917    124
       2757.39   6.900     92
       2756.29   6.897     86
    

in CDCl3

  • cb02232829_13cnmr_0

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