S-Benzoyl-N-(o-hydroxybenzylidene)thiohydroxylamine
Product Name S-Benzoyl-N-(o-hydroxybenzylidene)thiohydroxylamine
MFC14H11NO2S
MW257.30764
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MS-NW-7306 S-benzoyl-N-(o-hydroxybenzylidene)thiohydroxylamine C14H11NO2S (Mass of molecular ion: 257)
Source Temperature: 160 °C Sample Temperature: 140 °C Direct, 75 eV
17.0 1.5 18.0 5.4 27.0 3.3 28.0 3.2 37.0 1.7 38.0 3.5 39.0 12.5 45.0 1.8 50.0 9.2 51.0 24.6 52.0 3.1 53.0 2.2 62.0 1.7 63.0 5.7 64.0 4.3 65.0 6.5 66.0 2.2 69.0 1.1 74.0 2.4 75.0 2.6 76.0 3.1 77.0 57.1 78.0 4.6 81.0 1.1 90.0 2.1 91.0 5.0 92.0 1.4 93.0 2.2 97.0 1.7 102.0 1.2 105.0 100.0 106.0 7.9 119.0 2.2 120.0 1.0 121.0 1.6 136.0 3.9 152.0 1.1 225.0 1.7 257.0 4.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H11 N O2 S 0.015 g : 0.5 ml CDCl3 S-benzoyl-N-(o-hydroxybenzylidene)thiohydroxylamine Assign. Shift(ppm)
A 12.09 B 8.815 C 7.926 D 7.636 E 7.513 F 7.370 G 7.26 J 7.061 K 6.920
Hz ppm Int.
4831.20 12.089 387 3521.93 8.813 390 3173.18 7.940 37 3171.53 7.936 213 3170.98 7.935 153 3170.25 7.933 275 3169.51 7.931 109 3169.15 7.930 99 3168.60 7.929 85 3165.12 7.920 76 3163.10 7.915 291 3161.82 7.912 261 3160.90 7.910 64 3060.53 7.659 38 3059.25 7.655 73 3057.96 7.652 42 3053.75 7.642 48 3052.47 7.638 78 3051.92 7.637 139 3050.09 7.632 55 3045.69 7.621 71 3044.41 7.618 124 3043.13 7.615 64 3009.79 7.532 49 3008.51 7.528 159 3008.14 7.527 195 3007.59 7.526 109 3006.49 7.523 84 3003.01 7.515 33 3001.73 7.511 123 3001.18 7.510 147 3000.63 7.509 212 3000.08 7.507 250 2998.99 7.505 77 2994.59 7.494 53 2993.31 7.490 77 2992.76 7.489 134 2992.21 7.488 95 2991.11 7.485 33 2953.01 7.389 53 2951.54 7.386 56 2945.68 7.371 64 2944.58 7.368 94 2943.30 7.365 73 2937.44 7.351 63 2935.98 7.347 67 2902.27 7.263 134 2900.99 7.259 1000 2894.76 7.244 125 2892.93 7.239 118 2825.71 7.071 129 2825.16 7.070 126 2824.61 7.068 136 2817.28 7.050 114 2816.73 7.048 109 2816.18 7.047 116 2772.22 6.937 99 2771.13 6.934 102 2765.08 6.919 122 2764.72 6.918 119 2763.98 6.917 124 2757.39 6.900 92 2756.29 6.897 86
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