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MassMS-NW-0696 n-nitrosodiisobutylamine C8H18N2O (Mass of molecular ion: 158)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 3.5 18.0 4.2 27.0 16.7 28.0 7.0 29.0 31.2 30.0 47.9 31.0 1.1 32.0 1.0 39.0 13.7 40.0 2.2 41.0 55.8 42.0 61.6 43.0 97.5 44.0 5.5 53.0 1.4 54.0 1.1 55.0 14.7 56.0 22.6 57.0 100.0 58.0 5.1 68.0 1.2 70.0 6.2 71.0 1.1 72.0 4.7 73.0 12.8 74.0 1.0 84.0 57.4 85.0 14.1 86.0 19.0 87.0 1.4 99.0 1.2 103.0 10.0 115.0 24.6 116.0 1.8 141.0 5.1 158.0 5.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H18 N2 O 0.05 ml : 0.5 ml CDCl3 N-nitrosodiisobutylamine 
Assign. Shift(ppm)
A 3.907 B 3.405 C 2.12 D 2.04 E 0.960 F 0.863 J(A,C)=7.6HZ J(B,D)=7.6HZ J(C,E)=6.7HZ J(D,F)=6.8HZ
Hz ppm Int.1565.31 3.917 427 1557.74 3.898 430 1364.75 3.415 434 1357.18 3.396 430 862.43 2.158 30 855.10 2.140 59 848.39 2.123 78 841.67 2.107 63 834.96 2.090 35 834.23 2.088 33 828.98 2.075 34 828.37 2.073 34 821.66 2.056 61 814.94 2.040 79 808.11 2.023 63 801.39 2.006 30 800.66 2.004 31 386.96 0.969 1000 380.25 0.952 930 348.14 0.872 976 341.31 0.855 919
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
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