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MS-NW-9896 dibutyltin dibromide C8H18Br2Sn (Mass of molecular ion: 392)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.4 29.0 14.6 39.0 2.1 41.0 18.4 55.0 1.7 56.0 2.4 57.0 100.0 58.0 4.8 119.0 1.3 120.0 1.2 121.0 1.5 153.0 1.1 155.0 1.6 195.0 2.0 196.0 1.0 197.0 5.0 198.0 2.1 199.0 7.4 200.0 1.1 201.0 4.8 203.0 1.4 252.0 1.0 254.0 2.4 255.0 1.7 256.0 3.5 257.0 1.2 258.0 2.2 289.0 1.7 291.0 2.7 293.0 2.1 311.0 1.0 312.0 1.0 313.0 1.2 331.0 1.7 333.0 5.4 334.0 2.7 335.0 9.6 336.0 2.9 337.0 9.3 338.0 1.3 339.0 4.7 341.0 1.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H18 Br2 Sn 0.05 ml : 0.5 ml CDCl3 dibutyltin dibromide Assign. Shift(ppm)
A 1.907 B 1.777 C 1.432 D 0.959
Hz ppm Int.
771.24 1.930 119 764.04 1.912 229 755.86 1.892 220 744.63 1.864 39 724.24 1.813 91 716.92 1.794 143 715.21 1.790 129 709.23 1.775 179 708.37 1.773 169 701.29 1.755 140 693.85 1.737 57 590.70 1.479 59 583.25 1.460 186 575.68 1.441 289 568.36 1.423 301 561.16 1.405 192 553.96 1.387 60 390.38 0.977 589 383.06 0.959 1000 375.61 0.940 531
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