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4'-Hydroxyacetophenone

Product Name 4'-Hydroxyacetophenone

CAS99-93-4

MFC8H8O2

MW136.15

¹³CNMR

Mass

MS-NW-8737          
4'-hydroxyacetophenone
C8H8O2              (Mass of molecular ion:    136)

   Source Temperature: 290 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       4.2
      27.0       1.0
      38.0       2.1
      39.0      11.8
      43.0       7.3
      50.0       1.8
      51.0       2.2
      53.0       2.8
      62.0       1.8
      63.0       4.2
      64.0       2.4
      65.0      22.3
      66.0       2.2
      77.0       2.4
      92.0       1.7
      93.0      33.2
      94.0       3.0
     107.0       1.1
     121.0     100.0
     122.0       7.9
     136.0      33.4
     137.0       3.1

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₈ O₂	0.040 g : 0.5 ml CDCl₃
4'-hydroxyacetophenone

    Assign.     Shift(ppm)

      A             8.69
      B             7.925
      C             6.985
      D             2.601

     Hz     ppm     Int.

   3472.17   8.689     33
   3174.80   7.944     42
   3172.00   7.937    277
   3169.92   7.932     88
   3165.28   7.921     96
   3163.21   7.915    284
   3160.40   7.908     33
   2798.71   7.003     45
   2795.90   6.996    296
   2793.82   6.991     89
   2789.06   6.979     94
   2786.99   6.974    276
   2784.18   6.967     31
   1039.79   2.602   1000

¹H NMR	89.56 MHz
C₈ H₈ O₂	0.032 g : 0.5 ml CDCl₃
4'-hydroxyacetophenone

    Assign.     Shift(ppm)

      A             8.5
      B             7.915
      C             6.974
      D             2.593

     Hz     ppm     Int.

    758.88   8.474     25
    716.44   8.000     32
    713.63   7.969    194
    711.56   7.946     64
    709.06   7.918     24
    706.81   7.893     81
    704.69   7.869    227
    702.00   7.839     31
    631.38   7.050     38
    628.56   7.019    238
    626.44   6.995     70
    621.75   6.943     69
    619.63   6.919    186
    616.94   6.889     24
    232.25   2.594   1000

in CDCl3

KBr disc

nujol mull

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