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99-64-9

3-(Dimethylamino)benzoic acid

Product Name 3-(Dimethylamino)benzoic acid

CAS99-64-9

MFC9H11NO2

MW165.19

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  • 99-64-9_ms
    Mass

    MS-NW-3810          
    m-(dimethylamino)benzoic acid
    C9H11NO2            (Mass of molecular ion:    165)
    

       Source Temperature: 270 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       2.6
          27.0       1.2
          28.0       1.0
          38.0       1.1
          39.0       3.8
          42.0       7.4
          43.0       1.0
          44.0       3.1
          45.0       1.1
          50.0       3.5
          51.0       4.0
          52.0       1.5
          59.5       1.1
          63.0       3.2
          64.0       1.1
          65.0       5.9
          73.5       3.3
          74.0       1.8
          75.0       1.7
          76.0       1.9
          77.0       7.7
          78.0       3.3
          79.0       3.0
          82.5       2.0
          90.0       1.0
          91.0       2.9
          92.0       1.6
          93.0       1.5
         103.0       1.4
         104.0       3.9
         105.0       2.8
         118.0       5.3
         119.0       2.2
         120.0       3.4
         121.0       2.7
         132.0       1.0
         148.0       5.9
         149.0       5.9
         150.0       1.7
         164.0     100.0
         165.0      87.4
         166.0       9.3
    

400 MHz in DMSO-d6

  • 99-64-9_1hnmr

    1H NMR 399.65 MHz
    C9 H11 N O2 0.040 g : 0.5 ml DMSO-d6
    m-(dimethylamino)benzoic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.30 B 7.28 C 7.27 D 6.957 E 2.936

         Hz     ppm     Int.
    

       2925.17   7.320     24
       2917.85   7.302     72
       2910.16   7.282    178
       2908.45   7.278    140
       2902.59   7.263     23
       2901.12   7.260     26
       2786.74   6.973     30
       2784.30   6.967     40
       2782.23   6.962     29
       2779.30   6.955     28
       2777.59   6.951     28
       2776.37   6.948     31
       2774.78   6.944     27
       1173.58   2.937   1000
    

CCl4 solution

  • 99-64-9_ir1_3

KBr disc

  • 99-64-9_ir2_2

nujol mull

  • 99-64-9_ir3