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99-54-7

3,4-Dichloronitrobenzene

Product Name 3,4-Dichloronitrobenzene

CAS99-54-7

MFC6H3Cl2NO2

MW192

More

  • 99-54-7_ms
    Mass

    MS-NW-1663          
    1,2-dichloro-4-nitrobenzene
    C6H3Cl2NO2          (Mass of molecular ion:    191)
    

       Source Temperature: 250 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          18.0       2.5
          30.0      45.6
          35.0       1.0
          36.0       2.0
          37.0       8.9
          38.0       4.7
          39.0       1.3
          46.0       1.0
          47.0       1.5
          49.0       4.9
          50.0      14.9
          51.0       3.1
          54.5       1.0
          60.0       2.1
          61.0       5.6
          62.0       4.7
          63.0       6.0
          71.0       1.0
          72.0       3.5
          73.0      14.6
          74.0      52.2
          75.0      42.8
          76.0       3.1
          83.0       2.1
          84.0      15.1
          85.0      10.0
          86.0       5.5
          87.0       3.5
          88.0       1.0
          97.0       2.6
          98.0       1.3
         107.0       2.2
         108.0       3.4
         109.0      85.4
         110.0      19.0
         111.0      27.3
         112.0       6.0
         119.0       2.1
         121.0       1.3
         124.0       1.2
         126.0       1.4
         133.0      48.6
         134.0       2.8
         135.0      31.2
         136.0       1.8
         137.0       5.0
         144.0       1.5
         145.0     100.0
         146.0       7.4
         147.0      62.3
         148.0       4.4
         149.0      10.2
         161.0      36.0
         162.0       2.5
         163.0      22.9
         164.0       1.5
         165.0       3.8
         175.0       2.0
         177.0       1.3
         191.0      95.9
         192.0       6.9
         193.0      60.7
         194.0       4.3
         195.0      10.0
    

90 MHz in CDCl3

400 MHz in CDCl3

  • 99-54-7_1hnmr

    1H NMR 89.56 MHz
    C6 H3 Cl2 N O2 0.05 ml : 0.5 ml CDCl3
    1,2-dichloro-4-nitrobenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.341 B 8.084 C 7.654 J(A,B)=2.5HZ J(B,C)=8.8HZ

         Hz     ppm     Int.
    

        748.38   8.357    779
        745.88   8.329    919
        730.44   8.156    471
        727.88   8.128    352
        721.63   8.058    678
        719.06   8.029    572
        688.88   7.692   1000
        680.13   7.595    655
    

  • 99-54-7_1hnmr_2

    1H NMR 399.65 MHz
    C6 H3 Cl2 N O2 0.042 g : 0.5 ml CDCl3
    1,2-dichloro-4-nitrobenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.351 B 8.095 C 7.656

         Hz     ppm     Int.
    

       3338.75   8.355    922
       3336.18   8.348    965
       3241.33   8.111    528
       3238.65   8.104    496
       3232.42   8.089    571
       3229.86   8.082    557
       3068.12   7.678     22
       3064.09   7.667   1000
       3059.69   7.656     30
       3058.59   7.654     33
       3055.18   7.645    931
    

in CDCl3

  • 99-54-7_13cnmr

CCl4 solution

  • 99-54-7_ir1_4

KBr disc

  • 99-54-7_ir2_3

liquid film

  • 99-54-7_ir3_2

nujol mull

  • 99-54-7_ir4_1

4880 A,100M,powder

  • 99-54-7_raman