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3-Dimethylaminophenol

Product Name 3-Dimethylaminophenol

CAS99-07-0

MFC8H11NO

MW137.18

¹³CNMR

Mass

MS-NW-1243          
m-(dimethylamino)phenol
C8H11NO             (Mass of molecular ion:    137)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       3.1
      18.0       1.2
      27.0       2.1
      28.0       1.6
      30.0       1.2
      38.0       2.0
      39.0       8.4
      40.0       1.1
      41.0       1.6
      42.0       7.9
      43.0       1.4
      44.0       6.4
      50.0       1.2
      51.0       2.2
      52.0       1.9
      53.0       1.6
      55.0       1.2
      60.0       1.0
      62.0       1.1
      63.0       3.1
      64.0       1.8
      65.0       9.3
      66.0       3.5
      67.0       2.0
      68.0       2.7
      68.5       3.3
      77.0       2.3
      78.0       1.0
      79.0       1.1
      81.0       1.2
      91.0       2.4
      92.0       1.9
      93.0       5.5
      94.0       7.9
      95.0       2.2
     107.0       2.3
     108.0       6.3
     120.0       5.3
     121.0      10.3
     122.0       6.3
     123.0       2.5
     134.0       1.7
     136.0      98.4
     137.0     100.0
     138.0       8.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₁ N O	0.046 g : 0.5 ml CDCl₃
m-(dimethylamino)phenol

    Assign.     Shift(ppm)

      A             7.05
      B     *1      6.35
      C     *1      6.32
      D             6.20
      E             6.18
      F             2.814

     Hz     ppm     Int.

    640.13   7.148     29
    631.75   7.054     60
    623.44   6.962     40
    572.94   6.398     31
    572.00   6.387     42
    570.69   6.373     61
    569.81   6.363     74
    564.75   6.306     25
    562.69   6.283     50
    561.63   6.271     53
    560.38   6.258     60
    559.44   6.247     47
    557.25   6.223     53
    555.06   6.198     84
    554.06   6.187     67
    553.00   6.175     90
    252.06   2.815   1000
    248.56   2.776     29
    247.88   2.768     29

in CDCl3

KBr disc

nujol mull

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