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MS-NW-6901 N-lauroyl-N-methylglycine C15H29NO3 (Mass of molecular ion: 271)
Source Temperature: 240 °C Sample Temperature: 150 °C Direct, 75 eV
15.0 1.9 18.0 1.5 27.0 9.3 28.0 4.1 29.0 16.3 30.0 1.9 31.0 1.3 39.0 6.0 40.0 1.5 41.0 33.7 42.0 16.3 43.0 31.6 44.0 81.6 45.0 6.3 46.0 1.9 53.0 2.4 54.0 2.1 55.0 24.4 56.0 5.1 57.0 21.0 58.0 3.5 60.0 2.4 67.0 3.9 68.0 1.8 69.0 9.6 70.0 2.5 71.0 9.7 72.0 3.8 73.0 3.3 79.0 1.1 81.0 3.2 82.0 1.0 83.0 5.2 84.0 3.2 85.0 5.5 86.0 4.7 87.0 17.1 88.0 10.3 89.0 22.9 90.0 26.1 91.0 1.4 95.0 3.7 97.0 3.2 98.0 6.6 99.0 1.2 100.0 8.6 101.0 2.5 103.0 1.3 109.0 1.9 111.0 1.1 112.0 1.2 113.0 22.4 114.0 4.2 115.0 1.0 126.0 3.4 127.0 1.3 129.0 1.0 131.0 100.0 132.0 7.0 142.0 1.1 144.0 18.1 145.0 2.4 158.0 2.9 172.0 1.0 183.0 4.4 184.0 1.5 186.0 1.6 200.0 1.5 227.0 2.6 228.0 1.1 271.0 3.9 272.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H29 N O3 0.044 g : 0.5 ml CDCl3 N-lauroyl-N-methylglycine Assign. Shift(ppm)
A 10.5 B *1 4.148 C *1 4.064 D *2 3.098 E *2 2.988 F *3 2.394 G *3 2.268 J *4 1.64 K *4 1.61 L 1.42 to 1.190 M 0.89
Hz ppm Int.
1658.02 4.149 267 1624.50 4.065 72 1238.39 3.099 677 1194.25 2.989 143 964.74 2.414 94 957.23 2.396 117 949.35 2.376 101 661.05 1.655 54 654.64 1.639 80 654.27 1.638 80 647.13 1.620 67 639.62 1.601 32 521.84 1.306 235 505.54 1.265 1000 361.02 0.904 184 354.24 0.887 536 347.28 0.869 207
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