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Bis(dimethylthiocarbamyl) sulfide

Product Name Bis(dimethylthiocarbamyl) sulfide

CAS97-74-5

MFC6H12N2S3

MW208.37

¹³CNMR

Mass

MS-NW-5649          
tetramethylthiuram monosulfide
C6H12N2S3           (Mass of molecular ion:    208)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      15.0       3.1
      18.0       1.6
      28.0       1.7
      42.0       7.7
      43.0       1.4
      44.0       6.9
      45.0       1.8
      47.0       2.2
      56.0       2.5
      72.0       2.9
      73.0       7.6
      74.0       1.0
      76.0       1.5
      77.0       2.7
      88.0     100.0
      89.0       5.9
      90.0       4.5
     120.0       1.7
     176.0       1.2
     208.0      17.0
     209.0       1.8
     210.0       2.6

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₂ N₂ S₃	0.047 g : 0.5 ml CDCl₃
tetramethylthiuram monosulfide

    Assign.     Shift(ppm)

      A     *1      3.523
      B     *1      3.440

     Hz     ppm     Int.

    324.31   3.622     30
    322.88   3.606     32
    322.56   3.602     34
    322.13   3.597     38
    321.38   3.589     44
    320.81   3.583     49
    320.38   3.578     52
    315.56   3.524    986
    308.13   3.441   1000
    301.75   3.370     40

in CDCl3

CCl4 solution

KBr disc

nujol mull

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