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MS-NW-0589 3,4-dichlorotoluene C7H6Cl2 (Mass of molecular ion: 160)
Source Temperature: 280 °C Sample Temperature: 170 °C Reservoir, 75 eV
37.0 1.4 38.0 1.6 39.0 5.7 43.0 2.3 44.0 5.4 49.0 1.1 50.0 3.3 51.0 2.3 61.0 2.7 62.0 8.0 63.0 11.2 64.0 1.5 65.0 1.1 73.0 4.7 74.0 1.9 75.0 2.5 84.0 1.1 85.0 1.4 86.0 1.4 87.0 1.7 89.0 17.3 90.0 3.5 97.0 1.7 99.0 5.3 101.0 1.6 123.0 3.8 124.0 1.7 125.0 100.0 126.0 8.3 127.0 32.3 128.0 2.6 133.0 1.1 159.0 9.3 160.0 48.3 161.0 9.8 162.0 30.7 163.0 3.1 164.0 5.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H6 Cl2 0.04 ml : 0.5 ml CDCl3 3,4-dichlorotoluene Assign. Shift(ppm)
A 7.27 B 7.24 C 6.975 D 2.289
Hz ppm Int.
656.69 7.333 176 648.31 7.239 442 647.56 7.231 211 646.88 7.223 176 629.75 7.032 46 629.13 7.025 127 628.44 7.017 134 627.00 7.001 105 626.38 6.994 106 625.75 6.987 40 621.06 6.935 70 620.38 6.927 76 619.63 6.919 51 618.94 6.911 69 618.25 6.904 69 617.63 6.897 27 205.13 2.291 1000
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