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MassMS-NW-1687 3,4-xylenol C8H10O (Mass of molecular ion: 122)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 6.3 38.0 2.0 39.0 10.4 40.0 1.4 41.0 3.9 43.0 2.2 45.0 1.0 50.0 3.7 51.0 8.4 52.0 3.4 53.0 5.4 55.0 2.5 59.0 1.0 60.0 2.6 61.0 1.7 62.0 1.3 63.0 3.2 65.0 5.2 66.0 1.4 67.0 1.1 77.0 20.3 78.0 4.6 79.0 8.1 81.0 1.1 91.0 11.4 92.0 1.4 93.0 2.8 94.0 1.6 103.0 2.6 104.0 1.5 105.0 2.0 107.0 100.0 108.0 7.9 120.0 1.9 121.0 46.4 122.0 99.8 123.0 8.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H10 O 12.2 mg : 0.5 ml CDCl3 3,4-xylenol 
Assign. Shift(ppm)
A 6.978 B 6.640 C 6.575 D 4.7 E *1 2.205 F *1 2.176
Hz ppm Int.2793.33 6.990 138 2785.52 6.970 152 2785.16 6.969 156 2655.27 6.644 138 2652.83 6.638 171 2652.47 6.637 172 2633.06 6.589 103 2630.25 6.582 89 2624.88 6.568 95 2622.19 6.562 82 881.35 2.206 949 875.00 2.190 28 874.27 2.188 29 873.78 2.187 30 873.41 2.186 30 869.63 2.176 1000
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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