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MS-NW-9100 o-aminophenol C6H7NO (Mass of molecular ion: 109)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 2.0 27.0 2.7 28.0 4.0 31.0 1.6 38.0 1.6 39.0 3.2 40.0 1.5 40.5 1.7 41.0 2.1 50.0 1.6 51.0 2.6 52.0 4.4 53.0 7.1 54.0 2.8 54.5 3.1 55.0 1.2 63.0 3.8 64.0 6.1 65.0 1.7 80.0 30.5 81.0 6.1 91.0 1.7 92.0 1.2 108.0 8.8 109.0 100.0 110.0 7.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H7 N O 0.041 g : 0.5 ml DMSO-d6 o-aminophenol Assign. Shift(ppm)
A 8.9 B 6.649 C 6.587 D 6.543 E 6.400 F 4.4
Hz ppm Int.
2662.20 6.662 670 2660.83 6.658 716 2657.17 6.649 61 2654.42 6.642 783 2653.05 6.639 825 2638.70 6.603 413 2637.02 6.599 494 2634.28 6.592 55 2631.07 6.584 1000 2629.24 6.579 988 2625.12 6.569 51 2624.66 6.568 51 2622.07 6.561 560 2620.70 6.558 550 2617.65 6.550 57 2614.90 6.543 757 2613.53 6.540 684 2607.27 6.524 354 2605.74 6.521 320 2565.77 6.421 487 2563.78 6.416 481 2558.44 6.402 599 2557.98 6.401 578 2556.61 6.398 591 2550.81 6.383 347 2548.98 6.379 331 1778.87 4.452 139
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