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MassMS-NW-5019 o-phenetidine C8H11NO (Mass of molecular ion: 137)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 2.8 26.0 2.7 27.0 10.4 28.0 5.8 29.0 4.5 38.0 1.9 39.0 7.1 40.0 1.1 41.0 2.5 42.0 1.1 50.0 2.4 51.0 5.2 52.0 9.4 53.0 15.3 54.0 3.5 63.0 3.2 64.0 3.4 65.0 9.5 66.0 2.0 77.0 1.0 78.0 2.1 79.0 2.1 80.0 69.8 81.0 6.8 91.0 2.4 92.0 5.6 93.0 2.7 94.0 1.7 108.0 100.0 109.0 65.9 110.0 4.9 122.0 1.9 136.0 1.0 137.0 84.0 138.0 8.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N O 0.02 ml : 0.5 ml CDCl3 o-phenetidine 
Assign. Shift(ppm)
A 6.55 to 6.89 B 4.022 C 3.70 D 1.405
Hz ppm Int.609.06 6.801 53 608.31 6.793 81 606.94 6.777 31 606.63 6.774 31 604.31 6.748 127 602.63 6.729 772 601.38 6.715 691 600.94 6.710 774 599.50 6.694 207 597.25 6.669 45 595.31 6.648 85 594.69 6.641 72 371.13 4.144 118 364.06 4.065 401 357.06 3.987 423 350.19 3.911 143 330.94 3.696 953 132.56 1.481 482 125.63 1.403 1000 118.63 1.325 420
in CDCl3
CCl4 solution
liquid film
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