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MS-NW-0553 N-ethyl-o-toluidine C9H13N (Mass of molecular ion: 135)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.6 27.0 2.5 28.0 1.6 29.0 1.0 30.0 1.0 39.0 4.2 41.0 1.5 42.0 1.0 44.0 1.0 50.0 1.2 51.0 3.4 52.0 1.9 53.0 1.3 58.5 1.4 59.5 1.4 60.0 1.5 63.0 2.0 65.0 7.9 77.0 6.6 78.0 2.3 79.0 2.4 89.0 1.6 91.0 18.4 92.0 3.3 93.0 2.1 104.0 1.4 106.0 6.7 107.0 1.2 117.0 1.4 118.0 6.9 119.0 2.6 120.0 100.0 121.0 9.1 134.0 6.5 135.0 42.9 136.0 4.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H13 N 0.05 ml : 0.5 ml CDCl3 N-ethyl-o-toluidine Assign. Shift(ppm)
A 7.104 B 7.020 C 6.632 D 6.582 E 3.28 F 3.144 G 2.092 J 1.256
Hz ppm Int.
2848.14 7.127 57 2847.66 7.126 58 2846.56 7.123 65 2840.21 7.107 119 2839.60 7.106 118 2839.11 7.104 121 2838.62 7.103 123 2832.76 7.089 66 2832.28 7.087 66 2831.05 7.084 74 2810.18 7.032 117 2809.33 7.030 114 2802.86 7.014 128 2802.00 7.012 123 2658.33 6.652 91 2657.10 6.649 101 2650.88 6.634 163 2649.78 6.631 177 2643.55 6.615 78 2642.46 6.612 85 2634.77 6.593 163 2626.71 6.573 150 1267.46 3.172 150 1260.38 3.154 429 1253.30 3.136 424 1246.09 3.118 152 836.43 2.093 1000 509.28 1.275 538 502.20 1.257 938 495.00 1.239 489
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