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938-71-6More Spectrum > 4-CHLORO-2-NITROBENZYL CHLORIDE(938-71-6)13CNMR
4-CHLORO-2-NITROBENZYL CHLORIDE
Product Name 4-CHLORO-2-NITROBENZYL CHLORIDE
CAS938-71-6
MFC7H5Cl2NO2
MW206.03
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MS-IW-0577 4-chloro-1-chloromethyl-2-nitrobenzene C7H5Cl2NO2 (Mass of molecular ion: 205)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
29.0 2.4 30.0 5.9 36.0 1.1 37.0 1.9 38.0 4.2 39.0 12.1 44.0 1.0 49.0 2.7 50.0 11.2 51.0 14.2 52.0 2.4 60.0 1.1 61.0 7.4 62.0 23.7 63.0 51.5 64.0 4.9 65.0 1.2 72.0 1.9 73.0 22.7 74.0 8.1 75.0 28.5 76.0 10.7 77.0 16.8 78.0 13.8 79.0 1.8 83.0 1.0 84.0 2.0 85.0 6.8 86.0 9.9 87.0 14.2 88.0 6.5 89.0 76.4 90.0 76.6 91.0 14.9 92.0 1.1 96.0 1.3 97.0 10.3 98.0 3.1 99.0 76.7 100.0 6.0 101.0 23.9 102.0 2.8 106.0 2.8 107.0 1.9 109.0 2.5 110.0 4.3 111.0 30.6 112.0 53.4 113.0 18.4 114.0 31.3 115.0 5.4 116.0 5.1 117.0 1.1 123.0 78.5 124.0 43.4 125.0 36.3 126.0 79.1 127.0 9.0 128.0 21.6 129.0 1.8 133.0 16.6 134.0 1.4 135.0 11.0 137.0 1.9 138.0 2.0 139.0 26.8 140.0 12.3 141.0 10.0 142.0 33.0 143.0 2.8 144.0 9.7 145.0 1.0 146.0 1.6 148.0 1.0 152.0 1.7 153.0 9.3 154.0 3.8 155.0 3.8 156.0 1.2 158.0 7.7 159.0 17.4 160.0 19.9 161.0 12.4 162.0 10.5 163.0 2.6 164.0 1.6 170.0 100.0 171.0 8.5 172.0 32.5 173.0 2.9 205.0 2.4 207.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H5 Cl2 N O2 0.035 g : 0.5 ml CDCl3 4-chloro-1-chloromethyl-2-nitrobenzene Assign. Shift(ppm)
A 8.064 B 7.654 C 7.637 D 4.942
Hz ppm Int.
3223.63 8.067 217 3221.92 8.062 224 3066.28 7.673 65 3065.80 7.672 66 3057.86 7.652 337 3057.50 7.651 341 3054.69 7.644 309 3052.73 7.639 280 3046.39 7.623 58 3044.43 7.618 66 1975.10 4.943 1000
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