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MassMS-NW-1231 2-ethyl-4-methyl-2-imidazoline C6H12N2 (Mass of molecular ion: 112)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 7.4 18.0 2.7 26.0 5.0 27.0 20.1 28.0 33.8 29.0 21.7 30.0 8.4 32.0 1.1 38.0 1.2 39.0 8.6 40.0 3.7 41.0 24.1 42.0 21.8 43.0 6.0 44.0 33.3 45.0 1.7 48.0 4.1 48.5 1.0 52.0 2.6 53.0 1.6 54.0 28.8 55.0 7.4 56.0 37.9 57.0 9.9 58.0 3.9 67.0 1.9 68.0 24.5 69.0 100.0 70.0 12.1 71.0 1.1 72.0 6.3 73.0 17.3 81.0 1.8 82.0 29.0 83.0 55.8 84.0 4.4 86.0 1.3 95.0 5.5 96.0 3.4 97.0 69.6 98.0 5.1 99.0 1.3 100.0 1.1 101.0 1.2 109.0 3.6 110.0 2.4 111.0 16.3 112.0 58.8 113.0 4.6 123.0 1.8 125.0 3.0 137.0 2.2 138.0 1.4 139.0 7.5 140.0 1.4 152.0 1.8 154.0 3.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H12 N2 0.04 ml : 0.5 ml CDCl3 2-ethyl-4-methyl-2-imidazoline 
Assign. Shift(ppm)
A 4.2 B 3.94 C *1 3.69 D *1 3.15 E 2.23 F 1.19 G 1.17
Hz ppm Int.371.06 4.144 30 370.50 4.137 31 370.19 4.134 30 364.31 4.068 35 358.13 3.999 34 357.38 3.991 34 354.88 3.963 46 348.69 3.894 64 348.06 3.887 67 342.31 3.823 83 341.38 3.812 87 340.63 3.804 83 338.69 3.782 40 338.00 3.775 37 331.31 3.700 77 330.50 3.691 132 329.75 3.682 75 321.94 3.595 38 321.13 3.586 75 320.31 3.577 44 290.25 3.241 71 284.00 3.172 47 283.31 3.164 87 282.56 3.155 52 280.31 3.130 44 279.56 3.122 70 278.88 3.114 43 273.25 3.052 38 272.56 3.044 41 213.19 2.381 36 212.50 2.373 37 211.69 2.364 49 211.00 2.356 41 205.69 2.297 119 204.19 2.280 151 199.19 2.225 69 198.19 2.213 151 197.50 2.206 125 196.69 2.197 187 196.00 2.189 174 194.44 2.172 54 193.44 2.160 36 193.25 2.158 36 191.38 2.137 46 190.56 2.128 58 189.75 2.119 61 189.06 2.111 82 188.44 2.105 63 112.06 1.252 411 111.63 1.247 354 109.50 1.223 746 104.81 1.171 1000 104.06 1.162 852 103.38 1.155 943 99.75 1.114 57 98.63 1.102 36 97.50 1.089 173 96.94 1.083 294 96.25 1.075 228 93.75 1.047 33
CCl4 solution
liquid film
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