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MassMS-IW-3866 2-mercapto-N-(2-naphthyl)acetamide C12H11NOS (Mass of molecular ion: 217)
Source Temperature: 140 °C Sample Temperature: 120 °C Direct, 75 eV
39.0 1.6 45.0 1.3 47.0 6.3 50.0 1.1 51.0 1.7 62.0 1.4 63.0 3.5 65.0 1.7 74.0 1.0 75.0 1.7 77.0 2.0 88.0 1.4 89.0 3.3 101.0 1.1 113.0 2.0 114.0 3.6 115.0 29.6 116.0 6.7 126.0 2.3 127.0 9.4 128.0 2.6 129.0 1.1 140.0 3.7 141.0 3.2 142.0 11.7 143.0 100.0 144.0 14.8 145.0 1.0 156.0 2.0 169.0 6.7 170.0 4.0 173.0 3.2 174.0 6.3 175.0 1.2 184.0 4.3 185.0 2.0 217.0 72.7 218.0 10.5 219.0 4.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H11 N O S 0.040 g : 0.5 ml CDCl3 2-mercapto-N-(2-naphthyl)acetamide 
Assign. Shift(ppm)
A 8.76 B 8.185 C 7.76 D 7.75 E 7.474 F *1 7.43 G *1 7.39 J 3.379 K 2.038 J(J,K)=9.2HZ
Hz ppm Int.3501.59 8.762 122 3272.22 8.188 320 3270.26 8.183 331 3104.61 7.769 492 3101.68 7.761 222 3101.07 7.760 234 3100.59 7.759 232 3099.61 7.756 257 3095.95 7.747 582 3092.16 7.738 283 3091.80 7.737 289 3086.79 7.724 34 2992.43 7.488 238 2990.36 7.483 240 2983.64 7.466 222 2981.45 7.461 225 2979.49 7.456 121 2978.03 7.452 123 2972.66 7.439 225 2971.44 7.436 215 2970.09 7.432 117 2967.41 7.426 47 2964.84 7.419 228 2963.13 7.415 377 2961.55 7.411 252 2959.59 7.406 64 2956.30 7.398 141 2954.96 7.394 214 2953.74 7.391 226 2948.24 7.378 109 2946.90 7.374 98 1355.47 3.392 938 1346.31 3.369 1000 823.73 2.062 319 814.58 2.039 612 805.42 2.016 291
in CDCl3
KBr disc
nujol mull
