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MS-NW-4209 2-(2-aminoethoxy)ethanol C4H11NO2 (Mass of molecular ion: 105)
Source Temperature: 230 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.8 18.0 8.8 19.0 1.2 27.0 4.2 28.0 5.0 29.0 2.6 30.0 100.0 31.0 3.3 41.0 1.1 42.0 5.4 43.0 10.8 44.0 20.4 45.0 11.1 58.0 1.5 59.0 1.0 60.0 1.5 100.0 1.1
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C4 H11 N O2 0.05 ml : 0.5 ml CDCl3 2-(2-aminoethoxy)ethanol Assign. Shift(ppm)
A 3.701 B 3.563 C 3.520 D 2.872 E 2.8
Hz ppm Int.
1484.99 3.716 565 1482.79 3.711 230 1480.59 3.705 785 1479.25 3.702 526 1477.54 3.698 269 1475.59 3.693 867 1471.80 3.683 57 1434.81 3.591 31 1428.34 3.574 814 1426.51 3.570 267 1424.68 3.565 487 1423.34 3.562 792 1421.26 3.557 251 1418.95 3.551 602 1411.99 3.534 758 1406.98 3.521 1000 1401.73 3.508 857 1395.02 3.491 37 1153.08 2.886 468 1147.83 2.873 698 1142.82 2.860 476
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1H NMR 89.56 MHz C4 H11 N O2 0.04 ml : 0.5 ml CDCl3 2-(2-aminoethoxy)ethanol Assign. Shift(ppm)
A 3.70 B 3.57 C 3.52 D 2.878 E 2.64 400MHZ : HSP-44-769
Hz ppm Int.
338.31 3.778 188 336.56 3.758 231 334.88 3.740 303 333.25 3.721 359 332.50 3.713 374 331.38 3.701 424 328.94 3.673 758 328.25 3.666 781 323.44 3.612 810 322.63 3.603 751 321.88 3.595 382 320.69 3.581 601 319.13 3.564 414 318.31 3.555 387 316.00 3.529 1000 315.06 3.518 669 313.31 3.499 209 310.69 3.470 726 262.44 2.931 608 257.06 2.871 753 252.31 2.818 406 236.13 2.637 572
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