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N-Benzyl-N-ethylaniline

Product Name N-Benzyl-N-ethylaniline

CAS92-59-1

MFC15H17N

MW211.3

¹³CNMR

Mass

MS-NW-8491          
N-ethyl-N-phenylbenzylamine
C15H17N             (Mass of molecular ion:    211)

   Source Temperature: 260 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV

      27.0       1.8
      28.0       1.2
      29.0       1.8
      39.0       4.3
      41.0       1.4
      50.0       1.2
      51.0       7.3
      52.0       1.3
      63.0       2.0
      64.0       1.0
      65.0      11.0
      77.0      16.5
      78.0       2.4
      79.0       1.7
      89.0       1.5
      91.0     100.0
      92.0       8.5
     104.0       5.8
     105.0       2.0
     106.0       4.6
     118.0       1.2
     120.0       1.7
     134.0       7.6
     180.0       1.6
     182.0       1.2
     196.0      17.0
     197.0       2.7
     210.0       1.6
     211.0      22.7
     212.0       3.9

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₅ H₁₇ N	0.05 ml : 0.5 ml CDCl₃
N-ethyl-N-phenylbenzylamine

    Assign.     Shift(ppm)

      A             7.258
      B             7.207
      C             7.18
      D             7.15
      E             6.66
      F             6.64
      G             4.461
      J             3.418
      K             1.159

     Hz     ppm     Int.

   2909.91   7.282     97
   2908.81   7.279    138
   2907.35   7.275     69
   2902.34   7.263    247
   2901.49   7.261    329
   2900.51   7.258    249
   2896.36   7.248    134
   2894.41   7.243    380
   2883.30   7.215    418
   2876.34   7.198    298
   2871.46   7.185     87
   2869.38   7.180    190
   2865.72   7.171    157
   2864.01   7.167    141
   2862.18   7.162     93
   2861.57   7.161     97
   2859.01   7.154    348
   2857.30   7.150    367
   2854.98   7.144     67
   2852.17   7.137    115
   2850.10   7.132    312
   2847.66   7.126     49
   2669.68   6.681    294
   2668.70   6.678    396
   2661.74   6.661    284
   2660.77   6.658    445
   2659.79   6.656    374
   2657.35   6.650     61
   2654.54   6.643    168
   2653.56   6.640    253
   2647.22   6.624     83
   2646.24   6.622    124
   2645.39   6.620     70
   1783.08   4.462    674
   1376.71   3.445    148
   1369.63   3.428    419
   1362.55   3.410    420
   1355.47   3.392    149
    470.46   1.178    556
    463.38   1.160   1000
    459.47   1.150     41
    456.30   1.142    533

¹H NMR	89.56 MHz
C₁₅ H₁₇ N	0.04 ml : 0.5 ml CDCl₃
N-ethyl-N-phenylbenzylamine

    Assign.     Shift(ppm)

      A             7.25
      B             7.16
      C             6.76
      D             6.65
      E             4.495
      F             3.434
      G             1.186

     Hz     ppm     Int.

    652.38   7.285     79
    652.25   7.283     79
    651.81   7.278     80
    650.88   7.268    163
    649.00   7.247   1000
    645.50   7.208     89
    643.63   7.187    118
    642.06   7.170    150
    641.38   7.162    226
    639.38   7.140     39
    637.31   7.117     51
    634.38   7.084    172
    605.25   6.759     35
    602.44   6.727    304
    600.13   6.701     61
    595.31   6.648    181
    594.69   6.641    187
    593.63   6.629    129
    589.19   6.579     31
    588.00   6.566     47
    402.63   4.496    410
    319.69   3.570     60
    312.63   3.491    194
    305.63   3.413    208
    298.50   3.333     72
    113.06   1.263    290
    106.06   1.185    583
     99.00   1.106    248

in CDCl3

CCl4 solution

liquid film

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