(R,R)-(+)-N,N'-BIS(ALPHA-METHYLBENZYL)SULFAMIDE
Product Name (R,R)-(+)-N,N'-BIS(ALPHA-METHYLBENZYL)SULFAMIDE
CAS91410-68-3
MFC16H20N2O2S
MW304.41
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MassMS-NW-7622 (R,R)-(+)-N,N'-bis(alpha-methylbenzyl)sulfamide C16H20N2O2S (Mass of molecular ion: 304)
Source Temperature: 220 °C Sample Temperature: 190 °C Direct, 75 eV
15.0 2.7 18.0 1.2 27.0 6.9 28.0 9.4 38.0 1.4 39.0 6.8 41.0 2.4 42.0 22.5 43.0 2.8 44.0 10.3 48.0 2.7 50.0 5.5 51.0 17.8 52.0 4.6 53.0 2.3 63.0 2.8 64.0 2.6 65.0 4.3 74.0 1.3 75.0 1.5 76.0 2.9 77.0 37.2 78.0 14.1 79.0 22.9 80.0 1.8 89.0 1.3 91.0 9.4 92.0 2.4 93.0 1.5 102.0 1.0 103.0 10.3 104.0 32.7 105.0 100.0 106.0 71.3 107.0 5.7 118.0 4.0 119.0 7.7 120.0 29.8 121.0 3.2 123.0 1.2 137.0 1.9 168.0 2.7 185.0 33.4 186.0 3.2 187.0 1.8 199.0 14.2 200.0 1.8 210.0 2.7 289.0 40.5 290.0 7.6 291.0 2.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C16 H20 N2 O2 S 0.038 g : 0.5 ml CDCl3 (R,R)-(+)-N,N'-bis(alpha-methylbenzyl)sulfamide 
Assign. Shift(ppm)
A 7.3 to 7.14 B 4.53 C 4.40 D 1.453
Hz ppm Int.655.31 7.317 70 653.81 7.301 92 653.50 7.297 94 652.56 7.287 143 651.25 7.272 161 650.81 7.267 154 649.19 7.249 498 647.38 7.229 501 646.13 7.215 543 645.06 7.203 1000 643.06 7.181 716 639.81 7.144 232 638.50 7.130 135 636.88 7.112 98 634.88 7.089 114 633.31 7.072 65 409.56 4.574 88 409.13 4.569 90 408.88 4.566 90 408.56 4.562 90 408.06 4.557 93 406.56 4.540 113 405.94 4.533 112 405.56 4.529 112 402.63 4.496 86 400.38 4.471 164 396.13 4.424 53 393.94 4.399 178 387.50 4.327 115 133.50 1.491 777 130.00 1.452 133 126.94 1.418 746 122.56 1.369 57
in CDCl3
KBr disc
nujol mull
