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MassMS-NW-7729 1,2,3,5-tetraphenylbenzene C30H22 (Mass of molecular ion: 382)
Source Temperature: 190 °C Sample Temperature: 150 °C Direct, 75 eV
77.0 1.3 91.0 2.0 92.0 1.2 138.0 1.1 144.5 1.6 150.0 2.0 151.0 2.7 151.5 1.3 152.0 3.3 156.5 1.2 162.0 1.5 163.0 2.4 163.5 1.1 168.5 2.2 169.0 1.4 169.5 2.7 170.0 2.4 170.5 1.6 174.0 1.1 175.0 3.8 175.5 2.6 176.0 3.2 176.5 1.0 177.0 1.4 180.5 1.1 181.5 3.1 182.0 3.1 182.5 2.0 183.0 2.8 183.5 1.4 187.0 1.2 188.0 1.3 189.0 1.0 191.0 3.3 191.5 1.0 202.0 1.0 226.0 1.3 236.0 2.0 276.0 2.5 277.0 1.2 278.0 1.0 289.0 7.4 290.0 4.4 291.0 4.7 292.0 1.1 300.0 2.5 301.0 1.6 302.0 7.5 303.0 6.0 304.0 5.4 305.0 6.1 306.0 1.6 326.0 1.3 328.0 1.0 339.0 2.6 340.0 1.1 341.0 5.5 342.0 1.7 350.0 1.2 351.0 1.1 352.0 1.9 353.0 1.8 354.0 1.4 363.0 2.3 364.0 1.5 365.0 6.3 366.0 4.4 367.0 3.6 368.0 1.1 376.0 1.3 377.0 1.2 378.0 1.2 379.0 2.3 380.0 1.7 381.0 10.1 382.0 100.0 383.0 32.2 384.0 5.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C30 H22 0.036 g : 0.5 ml CDCl3 1,2,3,5-tetraphenylbenzene 
Assign. Shift(ppm)
A 7.70 B 7.682 C 7.443 D 7.356 E 7.15 to 7.14 F 6.98 G 6.87
Hz ppm Int.3081.91 7.712 165 3080.57 7.709 213 3078.61 7.704 82 3073.49 7.691 246 3072.39 7.688 246 3070.07 7.682 1000 2981.93 7.462 117 2980.22 7.458 56 2974.73 7.444 241 2973.51 7.441 141 2968.38 7.428 71 2966.92 7.424 146 2947.02 7.375 55 2945.68 7.371 97 2944.46 7.368 65 2940.43 7.358 45 2938.35 7.353 119 2936.28 7.348 41 2932.25 7.338 31 2931.03 7.334 48 2860.35 7.158 484 2858.15 7.152 807 2857.30 7.150 715 2854.49 7.143 854 2793.33 6.990 298 2791.50 6.985 309 2788.70 6.978 155 2788.09 6.977 150 2786.25 6.972 196 2748.78 6.878 184 2746.95 6.874 211 2743.90 6.866 107 2742.31 6.862 110 2741.82 6.861 111 2739.14 6.854 143
KBr disc
nujol mull
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