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MassMS-NW-0890 N,N-diethylcyclohexylamine C10H21N (Mass of molecular ion: 155)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 7.7 28.0 14.0 29.0 12.5 30.0 5.5 39.0 5.0 41.0 14.9 42.0 7.4 43.0 2.3 44.0 6.0 53.0 2.5 54.0 3.4 55.0 12.4 56.0 18.9 57.0 1.7 58.0 29.0 67.0 1.7 68.0 1.6 69.0 1.4 70.0 5.9 71.0 11.3 72.0 6.0 81.0 1.4 82.0 2.0 83.0 3.4 84.0 14.6 85.0 1.3 86.0 3.6 96.0 1.4 98.0 5.8 99.0 6.4 110.0 1.4 112.0 100.0 113.0 8.6 126.0 3.3 140.0 13.5 141.0 1.3 154.0 1.8 155.0 15.6 156.0 1.8
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C10 H21 N 0.05 ml : 0.5 ml CDCl3 N,N-diethylcyclohexylamine 
Assign. Shift(ppm)
A 2.540 B 2.48 C 1.79 D 1.620 E 1.21 F 1.10 G 1.026
Hz ppm Int.1026.12 2.568 219 1018.92 2.550 580 1011.72 2.532 590 1004.52 2.514 238 992.19 2.483 56 722.29 1.808 110 712.16 1.782 130 653.93 1.637 46 641.60 1.606 49 498.66 1.248 60 488.28 1.222 148 486.45 1.218 157 482.79 1.209 65 478.52 1.198 173 477.66 1.196 168 469.60 1.176 67 468.75 1.173 64 467.77 1.171 64 417.24 1.045 628 410.03 1.026 1000 402.83 1.008 599
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1H NMR 89.56 MHz C10 H21 N 0.04 ml : 0.5 ml CDCl3 N,N-diethylcyclohexylamine Assign. Shift(ppm)
A 2.532 B 2.53 C 1.78 D 1.18 E 1.03
Hz ppm Int.238.75 2.666 101 235.19 2.627 23 231.25 2.583 406 228.81 2.555 29 224.13 2.503 455 219.69 2.453 23 217.31 2.427 152 157.06 1.754 116 105.31 1.176 117 98.63 1.102 519 91.69 1.024 1000 84.38 0.943 359
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
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