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MassMS-NW-4686 alpha-bromo-2-xylene C8H9Br (Mass of molecular ion: 184)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
27.0 3.3 38.0 1.1 39.0 4.6 50.0 2.9 51.0 7.7 52.0 3.4 53.0 1.4 62.0 1.1 63.0 3.1 65.0 1.9 77.0 11.6 78.0 6.2 79.0 11.7 89.0 1.5 91.0 1.7 102.0 1.6 103.0 9.6 104.0 7.7 105.0 100.0 106.0 10.2 184.0 4.3 186.0 4.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 Br 0.04 ml : 0.5 ml CDCl3 alpha-bromo-2-xylene 
Assign. Shift(ppm)
A 2.399 B 4.494 C 6.97 to 7.39
Hz ppm Int.656.38 7.329 32 656.06 7.326 29 655.31 7.317 28 653.44 7.297 40 651.88 7.279 62 648.50 7.241 108 647.31 7.228 59 646.38 7.218 102 645.31 7.206 130 644.88 7.201 132 643.50 7.186 459 640.81 7.156 249 640.06 7.147 118 638.38 7.128 59 402.50 4.495 892 400.13 4.468 35 214.81 2.399 1000
in CDCl3
liquid film
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