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MassMS-NW-7783 2-methyl-8-nitroquinoline C10H8N2O2 (Mass of molecular ion: 188)
Source Temperature: 180 °C Sample Temperature: 140 °C Direct, 75 eV
15.0 1.6 18.0 2.4 26.0 2.4 27.0 8.9 28.0 3.5 30.0 12.5 37.0 3.3 38.0 6.7 39.0 31.5 40.0 2.0 41.0 1.9 43.0 4.4 46.0 2.0 49.0 1.2 50.0 14.0 51.0 16.9 52.0 6.5 53.0 2.7 57.5 1.3 61.0 3.4 62.0 10.4 63.0 22.5 64.0 7.5 65.0 9.1 66.0 1.0 73.0 1.2 74.0 12.3 75.0 11.5 76.0 7.5 77.0 17.7 78.0 4.9 86.0 2.4 87.0 4.9 88.0 6.9 89.0 20.0 90.0 4.3 91.0 2.0 98.0 1.7 99.0 2.0 100.0 3.7 101.0 3.0 102.0 6.1 103.0 26.4 104.0 4.5 113.0 6.5 114.0 9.2 115.0 79.1 116.0 20.2 117.0 1.6 127.0 4.3 128.0 5.0 129.0 2.2 130.0 100.0 131.0 10.6 140.0 14.6 141.0 7.2 142.0 25.8 143.0 3.1 158.0 28.4 159.0 3.3 172.0 1.8 188.0 66.3 189.0 8.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H8 N2 O2 0.045 g : 0.5 ml CDCl3 2-methyl-8-nitroquinoline 
Assign. Shift(ppm)
A 8.102 B *1 7.95 C *1 7.93 D 7.511 E 7.398 F 2.745
Hz ppm Int.3242.31 8.113 142 3233.76 8.092 151 3182.62 7.964 74 3181.40 7.961 93 3174.44 7.944 173 3173.22 7.940 179 3166.99 7.925 111 3165.65 7.922 79 3009.52 7.531 90 3001.71 7.511 125 2993.77 7.491 76 2960.82 7.409 164 2952.27 7.388 156 1097.29 2.746 1000
in CDCl3
KBr disc
nujol mull
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