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MS-NW-8910 dipiperidinomethane C11H22N2 (Mass of molecular ion: 182)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.3 27.0 3.8 28.0 9.6 29.0 9.5 30.0 9.3 39.0 3.5 40.0 1.0 41.0 9.7 42.0 15.0 43.0 9.9 44.0 12.4 53.0 1.4 54.0 1.9 55.0 8.8 56.0 13.1 57.0 11.1 58.0 1.2 67.0 2.1 68.0 2.0 69.0 2.8 70.0 6.3 82.0 1.7 84.0 35.8 85.0 19.1 86.0 1.5 94.0 1.4 95.0 1.9 96.0 3.9 97.0 8.5 98.0 100.0 99.0 8.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C11 H22 N2 0.04 ml : 0.5 ml CDCl3 dipiperidinomethane Assign. Shift(ppm)
A 2.828 B 2.46 to 2.35 C 1.67 to 1.33 CHEMICALLY EXCHENGING SYSTEM.
Hz ppm Int.
255.31 2.851 35 253.31 2.829 1000 251.25 2.806 30 218.94 2.445 251 215.88 2.411 419 210.38 2.350 376 148.75 1.661 59 147.94 1.652 54 147.00 1.642 51 143.13 1.599 166 142.19 1.588 155 133.50 1.491 479 131.81 1.472 630 130.63 1.459 448 125.88 1.406 78 123.63 1.381 60 123.13 1.375 61 120.75 1.349 40 119.94 1.340 35 119.50 1.335 36 118.88 1.328 36 118.44 1.323 35
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