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MassMS-NW-5117 phthaloyl dichloride C8H4Cl2O2 (Mass of molecular ion: 202)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 1.8 28.0 2.7 29.0 5.3 35.0 1.3 36.0 5.5 37.0 5.0 37.5 2.2 38.0 9.1 39.0 1.1 49.0 2.7 50.0 21.6 51.0 2.9 52.0 6.9 61.0 1.8 62.0 1.2 66.0 10.0 73.0 2.3 73.5 8.7 74.5 14.8 75.5 23.7 76.5 2.5 84.0 1.3 104.0 21.8 105.0 2.0 111.0 29.3 112.0 2.2 113.0 9.8 139.0 4.3 141.0 1.4 148.0 2.0 164.0 1.6 167.0 100.0 168.0 9.2 169.0 32.8 170.0 3.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H4 Cl2 O2 0.05 ml : 0.5 ml CDCl3 phthaloyl dichloride 
Assign. Shift(ppm)
A 7.940 B 7.787
Hz ppm Int.3181.76 7.962 172 3177.98 7.952 853 3174.68 7.944 798 3172.12 7.938 795 3168.95 7.930 1000 3164.92 7.920 227 3126.71 7.824 30 3120.48 7.809 164 3116.33 7.798 994 3113.16 7.790 702 3110.60 7.784 694 3107.30 7.776 764 3103.39 7.766 97 3097.66 7.751 23 3096.31 7.748 21
in CDCl3
liquid film
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