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2,6-Dimethylaniline

Product Name 2,6-Dimethylaniline

CAS87-62-7

MFC8H11N

MW121.18

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  • Mass 

    MS-NW-0578          
2,6-xylidine
C8H11N              (Mass of molecular ion:    121)


       Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV


          18.0       1.0
      27.0       3.1
      28.0       3.3
      30.0       2.0
      38.0       1.2
      39.0       6.3
      41.0       2.4
      42.0       3.4
      50.0       1.6
      51.0       4.2
      52.0       3.3
      53.0       4.5
      54.0       2.0
      58.5       1.7
      59.5       2.1
      60.5       1.9
      63.0       2.1
      65.0       4.2
      66.0       1.4
      77.0      11.9
      78.0       6.9
      79.0       4.9
      80.0       2.1
      91.0       8.3
      92.0       2.4
      93.0       3.6
      94.0       1.5
     102.0       1.1
     103.0       6.7
     104.0       4.6
     105.0       2.3
     106.0      56.5
     107.0       4.7
     118.0       2.4
     119.0       1.8
     120.0      53.1
     121.0     100.0
     122.0       9.1

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H11 N 0.04 ml : 0.5 ml CDCl3
    2,6-xylidine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             6.93
      B             6.62
      C             3.46
      D             2.155
  

         Hz     ppm     Int.


        624.63   6.975     73
    624.00   6.968     75
    623.38   6.961     62
    616.94   6.889    161
    616.38   6.883    145
    599.56   6.695     82
    593.19   6.624     48
    591.19   6.602     42
    584.88   6.531     28
    309.56   3.457     95
    193.00   2.155   1000

in CDCl3



liquid film





OXIDATION WITH PBA IN ETHANOL

OXIDATION WITH PERBENZOIC ACID IN DIOXANE





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