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MassMS-NW-0578 2,6-xylidine C8H11N (Mass of molecular ion: 121)
Source Temperature: 280 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 1.0 27.0 3.1 28.0 3.3 30.0 2.0 38.0 1.2 39.0 6.3 41.0 2.4 42.0 3.4 50.0 1.6 51.0 4.2 52.0 3.3 53.0 4.5 54.0 2.0 58.5 1.7 59.5 2.1 60.5 1.9 63.0 2.1 65.0 4.2 66.0 1.4 77.0 11.9 78.0 6.9 79.0 4.9 80.0 2.1 91.0 8.3 92.0 2.4 93.0 3.6 94.0 1.5 102.0 1.1 103.0 6.7 104.0 4.6 105.0 2.3 106.0 56.5 107.0 4.7 118.0 2.4 119.0 1.8 120.0 53.1 121.0 100.0 122.0 9.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N 0.04 ml : 0.5 ml CDCl3 2,6-xylidine 
Assign. Shift(ppm)
A 6.93 B 6.62 C 3.46 D 2.155
Hz ppm Int.624.63 6.975 73 624.00 6.968 75 623.38 6.961 62 616.94 6.889 161 616.38 6.883 145 599.56 6.695 82 593.19 6.624 48 591.19 6.602 42 584.88 6.531 28 309.56 3.457 95 193.00 2.155 1000
in CDCl3
liquid film
OXIDATION WITH PBA IN ETHANOL
OXIDATION WITH PERBENZOIC ACID IN DIOXANE
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