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MS-NW-9982 2-dibenzofuranol C12H8O2 (Mass of molecular ion: 184)
Source Temperature: 130 °C Sample Temperature: 100 °C Direct, 75 eV
18.0 2.1 50.0 1.1 51.0 3.9 63.0 2.9 63.5 1.2 64.0 2.5 74.0 1.5 75.0 2.2 76.0 1.1 77.0 2.5 77.5 1.3 92.0 10.5 92.5 1.3 101.0 2.0 102.0 3.8 126.0 2.5 127.0 6.5 128.0 12.3 129.0 1.7 155.0 6.3 156.0 2.9 183.0 2.9 184.0 100.0 185.0 13.1 186.0 1.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H8 O2 0.046 g : 0.5 ml DMSO-d6 2-dibenzofuranol Assign. Shift(ppm)
A 9.53 B 8.086 C 7.652 D 7.532 E 7.49 F 7.50 G 7.368 J 7.011
Hz ppm Int.
3808.14 9.529 345 3236.08 8.098 379 3235.47 8.096 386 3228.45 8.079 414 3227.69 8.077 394 3062.74 7.664 481 3054.50 7.643 626 3015.14 7.545 750 3011.47 7.536 38 3011.02 7.535 38 3006.29 7.523 923 3004.30 7.518 308 2998.20 7.503 428 2996.52 7.498 1000 2993.93 7.492 792 2990.11 7.482 288 2988.74 7.479 265 2951.97 7.387 313 2951.20 7.385 300 2948.91 7.379 32 2948.30 7.378 30 2947.85 7.377 31 2944.34 7.368 484 2943.73 7.366 466 2940.83 7.359 34 2937.01 7.349 241 2936.25 7.348 219 2807.46 7.025 459 2804.87 7.019 452 2801.67 7.011 32 2798.61 7.003 432 2796.02 6.997 421
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