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85-46-1

1-Naphthalenesulfonyl chloride

Product Name 1-Naphthalenesulfonyl chloride

CAS85-46-1

MFC10H7ClO2S

MW226.68

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  • 85-46-1_ms
    Mass 

    MS-NW-1977          
1-naphthalenesulfonyl chloride
C10H7ClO2S          (Mass of molecular ion:    226)


       Source Temperature: 230 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV


          18.0       3.2
      36.0       2.4
      39.0       1.8
      44.0       1.0
      48.0       5.0
      50.0       3.6
      51.0       5.6
      62.0       2.1
      63.0       7.9
      63.5       5.1
      64.0      10.8
      74.0       4.3
      75.0       6.1
      76.0       3.2
      77.0      10.2
      78.0       1.0
      81.0       1.2
      86.0       1.0
      87.0       2.1
      89.0       1.0
      98.0       1.1
      99.0       1.1
     100.0       1.1
     101.0       6.3
     102.0       1.8
     115.0       6.3
     125.0       1.1
     126.0      13.6
     127.0     100.0
     128.0      25.0
     129.0       2.3
     143.0       3.9
     147.0       2.4
     159.0       1.4
     162.0      32.1
     163.0       3.8
     164.0      10.4
     165.0       1.0
     175.0       3.9
     191.0      16.7
     192.0       1.9
     193.0       1.0
     206.0       2.1
     208.0       2.0
     226.0      29.2
     227.0       3.3
     228.0      11.0
     229.0       1.3
     252.0       1.4
     253.0       1.7
     254.0       1.1
     285.0       1.6
     286.0       5.5
     287.0       1.2

90 MHz in CDCl3

  • 85-46-1_1hnmr

    1H NMR 89.56 MHz
    C10 H7 Cl O2 S 0.042 g : 0.5 ml CDCl3
    1-naphthalenesulfonyl chloride
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             8.78
      B             8.354
      C             8.20
      D             8.00
      E     *1      7.77
      F     *1      7.71
      G             7.59
  

         Hz     ppm     Int.


        792.75   8.852    197
    791.94   8.843    343
    791.13   8.834    267
    790.50   8.827    372
    789.69   8.818    359
    788.19   8.801     47
    787.00   8.788     40
    786.50   8.782     44
    785.25   8.768    189
    784.31   8.758    237
    783.69   8.751    277
    782.88   8.742    425
    782.19   8.734    439
    781.38   8.725    261
    754.50   8.425     41
    753.00   8.408    562
    751.75   8.394    651
    749.19   8.366     47
    748.81   8.361     44
    748.50   8.358     44
    748.06   8.353     46
    745.56   8.325    658
    744.25   8.311    811
    742.00   8.285     56
    738.56   8.247    438
    735.38   8.212     42
    735.00   8.207     46
    734.56   8.202     40
    733.63   8.192     39
    732.88   8.184     48
    731.19   8.165    408
    730.31   8.155    581
    726.00   8.107     39
    721.00   8.051    248
    719.50   8.034    221
    718.06   8.018    198
    716.06   7.996     51
    715.75   7.992     53
    715.31   7.987     54
    713.63   7.969    529
    711.44   7.944    492
    708.44   7.911     44
    707.13   7.896    176
    705.19   7.874    264
    703.44   7.855     46
    702.56   7.845     40
    701.69   7.835     51
    700.13   7.818    618
    698.25   7.797    399
    696.81   7.781    205
    695.75   7.769     77
    694.06   7.750    638
    692.56   7.733    767
    691.81   7.725    802
    689.94   7.704    441
    686.06   7.661   1000
    684.81   7.647    492
    682.44   7.620     59
    681.88   7.614     53
    681.75   7.613     53
    680.94   7.604     40
    680.50   7.599     44
    678.50   7.576    703
    677.75   7.568    745
    675.69   7.545     46
    670.25   7.484    460

KBr disc

  • 85-46-1_ir1

  • 85-46-1_raman

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