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MS-NW-7880 4-methoxy-1-naphthol C11H10O2 (Mass of molecular ion: 174)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
15.0 1.4 18.0 1.1 28.0 1.1 38.0 1.0 39.0 2.4 50.0 4.1 51.0 7.3 52.0 1.5 53.0 1.8 57.5 1.0 62.0 2.2 63.0 4.3 65.0 1.7 65.5 2.0 74.0 3.0 75.0 4.5 76.0 6.9 77.0 19.6 78.0 1.6 86.0 1.4 87.0 5.0 88.0 1.6 89.0 2.2 91.0 3.8 101.0 2.3 102.0 7.9 103.0 18.1 104.0 4.3 105.0 13.3 106.0 2.1 113.0 1.5 114.0 1.9 115.0 5.9 116.0 1.0 129.0 1.0 130.0 3.2 131.0 23.8 132.0 2.5 145.0 3.1 159.0 100.0 160.0 11.6 161.0 1.1 173.0 5.8 174.0 85.5 175.0 10.8 176.0 1.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C11 H10 O2 0.039 g : 0.5 ml DMSO-d6 4-methoxy-1-naphthol Assign. Shift(ppm)
A 9.59 B *1 8.12 C *1 8.09 D *2 7.498 E *2 7.479 F 6.790 G 6.772 J 3.883 J(F,G)=8.2HZ
Hz ppm Int.
3834.53 9.595 378 3252.56 8.139 65 3251.95 8.137 69 3248.90 8.130 86 3246.77 8.125 51 3245.09 8.120 68 3242.95 8.115 79 3242.19 8.113 84 3239.75 8.107 84 3238.98 8.105 70 3236.85 8.100 69 3235.17 8.096 53 3233.03 8.090 99 3229.98 8.083 86 3229.37 8.081 68 2997.44 7.501 202 2994.69 7.494 113 2993.62 7.491 106 2991.49 7.486 114 2990.57 7.483 99 2987.67 7.476 191 2720.18 6.807 65 2712.10 6.787 303 2707.82 6.776 258 2699.58 6.755 58 1551.82 3.883 1000
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