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MS-NW-6471 2',4'-dimethoxyacetophenone C10H12O3 (Mass of molecular ion: 180)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.8 18.0 1.6 39.0 1.7 43.0 7.3 50.0 1.5 51.0 3.7 52.0 1.1 53.0 1.1 62.0 1.4 63.0 3.7 64.0 2.1 65.0 2.0 66.0 1.1 69.0 1.0 77.0 6.6 78.0 1.6 79.0 3.7 91.0 1.1 92.0 3.6 94.0 1.6 107.0 5.9 109.0 1.8 121.0 1.1 122.0 10.3 135.0 4.4 137.0 1.7 150.0 4.6 151.0 1.1 163.0 3.4 165.0 100.0 166.0 11.0 167.0 1.2 180.0 25.8 181.0 3.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H12 O3 0.048 g : 0.5 ml CDCl3 2',4'-dimethoxyacetophenone Assign. Shift(ppm)
A 7.815 B 6.51 C 6.45 D *1 3.882 E *1 3.841 F 2.564
Hz ppm Int.
704.81 7.870 74 703.88 7.860 51 696.69 7.780 62 695.75 7.769 83 588.44 6.571 51 586.13 6.545 80 578.00 6.454 206 576.56 6.438 43 347.75 3.883 624 344.06 3.842 745 229.63 2.564 1000
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