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MS-IW-2287 2-vinylnaphthalene C12H10 (Mass of molecular ion: 154)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
39.0 1.0 50.0 1.5 51.0 3.1 63.0 4.0 64.0 2.8 74.0 1.6 75.0 3.0 75.5 1.1 76.0 10.3 76.5 1.7 77.0 5.4 89.0 1.0 101.0 1.6 102.0 2.3 115.0 3.5 126.0 3.5 127.0 4.8 128.0 8.5 129.0 4.8 139.0 2.3 141.0 1.1 142.0 1.0 150.0 3.0 151.0 9.5 152.0 31.8 153.0 49.8 154.0 100.0 155.0 13.2 156.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H10 0.030 g : 0.5 ml CDCl3 2-vinylnaphthalene Assign. Shift(ppm)
A 7.79 to 7.77 B 7.728 C 7.622 D *1 7.44 E *1 7.42 F 6.867 G 5.859 J 5.321
Hz ppm Int.
3117.19 7.800 387 3114.87 7.794 672 3110.96 7.785 977 3107.91 7.777 729 3105.35 7.771 472 3102.17 7.763 737 3088.75 7.729 785 3050.90 7.634 527 3049.19 7.630 508 3042.36 7.613 390 3040.65 7.609 381 2983.40 7.466 117 2981.81 7.462 162 2976.56 7.448 466 2974.73 7.444 456 2973.14 7.440 563 2970.09 7.432 1000 2966.92 7.424 484 2965.58 7.421 460 2963.75 7.416 445 2958.37 7.403 149 2956.91 7.399 109 2759.03 6.904 335 2748.17 6.877 350 2741.46 6.860 367 2730.59 6.833 373 2350.22 5.881 688 2332.64 5.837 631 2132.32 5.336 668 2131.96 5.335 674 2121.09 5.308 656
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