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82358-61-0

CYANOMETHYLTRI-N-BUTYLPHOSPHONIUM CHLORIDE

Product Name CYANOMETHYLTRI-N-BUTYLPHOSPHONIUM CHLORIDE

CAS82358-61-0

MFC14H29ClNP

MW277.81

  • 82358-61-0_ms_1
    Mass

    MS-IW-8385          
    tributyl(cyanomethyl)phosphonium chloride
    C14H29ClNP          (Mass of molecular ion:    277)
    

       Source Temperature: 170 °C
       Sample Temperature: 170 °C
       Direct, 75 eV
    

          17.0       1.4
          18.0       7.9
          26.0       2.5
          27.0      12.4
          28.0       7.9
          29.0      35.5
          30.0       1.0
          35.0       3.3
          36.0      37.3
          37.0       1.2
          38.0      12.4
          39.0      10.9
          40.0       3.2
          41.0      46.6
          42.0       4.5
          43.0       4.5
          44.0       1.3
          45.0       4.4
          46.0       1.9
          47.0       4.9
          48.0       2.8
          49.0       1.2
          50.0       1.0
          51.0       1.8
          52.0       1.1
          53.0       4.3
          54.0       8.5
          55.0      29.9
          56.0      10.1
          57.0      11.6
          58.0       2.3
          59.0       9.7
          60.0       2.7
          61.0      30.1
          62.0      33.9
          63.0       3.2
          67.0       2.2
          68.0       1.2
          69.0       3.1
          70.0       1.5
          71.0       5.7
          72.0      37.0
          73.0      13.0
          74.0       4.8
          75.0      12.5
          76.0     100.0
          77.0       5.0
          78.0       6.4
          81.0       1.7
          82.0       1.9
          83.0       6.6
          85.0       3.8
          86.0       7.4
          87.0      30.1
          88.0       9.0
          89.0       9.3
          90.0      48.2
          91.0       3.2
          92.0       7.8
          95.0       1.3
          96.0       4.2
          97.0       2.3
          98.0       1.4
          99.0       2.7
         100.0      10.2
         101.0      94.3
         102.0      17.9
         103.0      10.7
         104.0      17.1
         105.0       2.0
         113.0       2.4
         114.0       7.8
         115.0      43.5
         116.0      27.0
         117.0       5.3
         118.0      21.9
         119.0       1.7
         120.0       3.5
         126.0       1.4
         127.0       1.7
         128.0      58.1
         129.0      38.3
         130.0       9.6
         131.0      14.8
         132.0       4.0
         134.0       2.3
         140.0       1.0
         141.0       1.1
         142.0       8.8
         143.0      36.0
         144.0       4.8
         145.0      14.8
         146.0       6.8
         147.0       2.5
         156.0      24.0
         157.0      18.6
         158.0       7.7
         159.0       2.4
         160.0       8.8
         161.0       2.3
         162.0       2.1
         170.0      18.5
         171.0       4.8
         173.0       8.1
         174.0       1.9
         184.0      19.1
         185.0      18.5
         186.0       4.0
         187.0      13.3
         188.0       1.6
         189.0       3.0
         198.0       1.2
         199.0       2.4
         201.0       1.3
         202.0       5.4
         203.0       1.2
         212.0      45.6
         213.0       6.9
         226.0       6.1
         240.0      11.5
         241.0      49.5
         242.0      15.2
         243.0       1.8
    

400 MHz in CDCl3

  • 82358-61-0_1hnmr_1

    1H NMR 399.65 MHz
    C14 H29 Cl N P 0.046 g : 0.5 ml CDCl3
    tributyl(cyanomethyl)phosphonium chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.061 B 2.679 C 1.681 D 1.557 E 1.001

         Hz     ppm     Int.
    

       2030.52   5.081    140
       2014.89   5.042    139
       1086.18   2.718     98
       1080.69   2.705     61
       1077.64   2.697     80
       1072.75   2.685    139
       1069.46   2.676    142
       1064.70   2.665     84
       1062.13   2.658     63
       1058.59   2.649     46
       1056.03   2.643    113
        686.28   1.718     61
        684.94   1.714     63
        678.47   1.698    113
        674.07   1.687     84
        670.65   1.679    128
        665.77   1.666     68
        662.48   1.658     98
        659.67   1.651     50
        654.42   1.638     38
        639.89   1.602     38
        632.69   1.584    134
        625.37   1.565    216
        618.04   1.547    202
        610.84   1.529    109
        407.10   1.019    496
        399.90   1.001   1000
        392.58   0.983    466
    

in CDCl3

  • 82358-61-0_13cnmr_1

KBr disc

  • 82358-61-0_ir1_2

nujol mull

  • 82358-61-0_ir2_1