-
MassMS-NW-5661 1,9-dichlorononane C9H18Cl2 (Mass of molecular ion: 196)
Source Temperature: 280 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 1.2 27.0 22.9 28.0 2.4 29.0 21.6 36.0 1.6 39.0 16.8 40.0 2.6 41.0 71.6 42.0 14.8 43.0 34.2 44.0 1.5 49.0 5.1 51.0 1.8 53.0 5.8 54.0 7.0 55.0 93.3 56.0 16.8 57.0 11.9 63.0 6.6 65.0 2.5 67.0 8.3 68.0 9.7 69.0 53.2 70.0 11.6 71.0 1.7 75.0 1.3 76.0 1.0 77.0 3.9 79.0 1.3 81.0 5.5 82.0 10.9 83.0 22.6 84.0 3.9 90.0 2.2 91.0 100.0 92.0 6.0 93.0 34.5 94.0 1.9 95.0 4.5 96.0 2.3 97.0 4.9 98.0 1.3 104.0 11.8 105.0 11.9 106.0 4.5 107.0 3.9 111.0 1.0 118.0 5.9 119.0 1.2 120.0 2.0 132.0 2.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H18 Cl2 0.04 ml : 0.5 ml CDCl3 1,9-dichlorononane 
Assign. Shift(ppm)
A 3.519 B 1.77 C 1.5 D 1.44 to 1.20 J(A,B)=6.6HZ.
Hz ppm Int.322.38 3.600 369 318.50 3.557 35 315.94 3.528 968 309.31 3.454 589 164.81 1.841 93 164.38 1.836 92 162.69 1.817 84 162.38 1.814 84 161.88 1.808 85 158.50 1.770 166 158.19 1.767 167 152.25 1.700 138 151.25 1.689 128 147.38 1.646 60 147.06 1.643 60 146.63 1.638 62 146.38 1.635 62 145.56 1.626 66 145.00 1.620 67 141.94 1.585 44 141.63 1.582 46 140.88 1.574 47 140.44 1.569 49 139.81 1.562 49 139.44 1.557 49 136.81 1.528 86 133.94 1.496 119 133.38 1.490 118 132.50 1.480 113 130.25 1.455 122 118.44 1.323 1000 109.50 1.223 31
in CDCl3
liquid film
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