Diethyl chlorophosphate

Mass

MS-KW-0098          
diethyl chlorophosphate
C4H10ClO3P          (Mass of molecular ion:    172)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.9
      26.0       4.0
      27.0      17.1
      28.0      12.0
      29.0      29.5
      30.0       1.3
      31.0      16.6
      36.0       1.8
      42.0       1.0
      43.0       6.8
      44.0       2.7
      45.0      31.5
      47.0       5.4
      63.0       2.2
      64.0       3.8
      65.0       8.6
      66.0       1.2
      81.0      21.9
      83.0       1.2
      91.0       7.4
      93.0       1.3
      99.0      13.9
     100.0      28.4
     101.0       9.1
     102.0       9.4
     103.0       1.6
     109.0      15.9
     117.0     100.0
     119.0      33.2
     127.0       6.9
     128.0      10.2
     129.0      31.4
     130.0       3.7
     131.0      10.7
     135.0       1.0
     137.0       2.9
     143.0       9.3
     144.0       2.2
     145.0      66.9
     146.0       2.3
     147.0      21.2
     157.0       1.9
     161.0       1.6
     173.0       2.2
     179.0       2.1
     180.0       1.2
     197.0       1.9
     225.0       1.1
     253.0       1.1
     263.0       1.0

Assign. Shift(ppm) A 4.282 B 1.419

     Hz     ppm     Int.

   1732.30   4.335     69
   1729.37   4.328    106
   1725.22   4.317     87
   1723.51   4.313    134
   1722.29   4.310    274
   1719.97   4.304    118
   1718.14   4.300     68
   1716.43   4.295    284
   1715.21   4.292    290
   1714.23   4.290    163
   1712.89   4.286    270
   1711.30   4.282     62
   1710.82   4.281     61
   1709.35   4.278    268
   1708.01   4.274    156
   1707.15   4.272    281
   1705.69   4.268    280
   1704.22   4.265     73
   1702.39   4.260    114
   1700.07   4.254    259
   1698.73   4.251    129
   1697.02   4.247     86
   1692.99   4.237     97
   1689.94   4.229     69
    574.95   1.439    633
    573.73   1.436    605
    571.29   1.430     98
    567.87   1.421   1000
    566.65   1.418    968
    562.50   1.408    100
    560.79   1.404    581
    559.57   1.401    593