2-ETHYL-2-PHENYLMALONAMIDE HYDRATE

Mass

MS-NW-6598          
2-ethyl-2-phenylmalonamide
C11H14N2O2 H2O      (Mass of molecular ion:    206)

   Source Temperature: 190 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      17.0       3.3
      18.0      14.3
      27.0       2.8
      28.0       1.9
      29.0       1.4
      38.0       1.0
      39.0       7.5
      41.0       5.8
      42.0       3.3
      43.0       5.8
      44.0      15.2
      50.0       2.8
      51.0       7.9
      52.0       2.1
      53.0       1.0
      62.0       2.0
      63.0       4.7
      64.0       1.3
      65.0       4.5
      74.0       3.7
      75.0       1.5
      76.0       1.9
      77.0      12.3
      78.0       4.9
      79.0       2.9
      89.0       5.5
      90.0       3.3
      91.0      33.7
      92.0       3.2
     102.0       2.6
     103.0      31.7
     104.0       5.3
     105.0       2.8
     106.0       1.4
     115.0      12.7
     116.0       9.6
     117.0      20.7
     118.0       5.7
     119.0       5.3
     120.0      18.1
     121.0       1.8
     130.0       7.1
     131.0       3.0
     132.0       1.0
     133.0       1.2
     134.0       1.5
     135.0       2.5
     142.0       3.8
     143.0       3.5
     144.0       1.4
     145.0      15.9
     146.0       5.0
     148.0      82.8
     149.0       8.8
     160.0       1.6
     161.0       4.8
     162.0       2.5
     163.0     100.0
     164.0      11.9

Assign. Shift(ppm) A *1 7.99 B *1 7.38 C 7.34 D 7.32 E 7.242 F 2.308 G 0.830

     Hz     ppm     Int.

   3194.70   7.994    310
   2950.68   7.384    319
   2942.26   7.363     55
   2940.80   7.359    120
   2938.60   7.353    182
   2936.28   7.348     95
   2932.01   7.337    883
   2930.66   7.334   1000
   2924.07   7.317    521
   2922.00   7.312    150
   2917.97   7.302     98
   2915.89   7.297    164
   2901.37   7.260    112
   2899.41   7.255    188
   2897.09   7.250    102
   2895.51   7.246     92
   2893.80   7.241    132
   2892.70   7.239    173
   2890.01   7.232     66
   2888.18   7.227     55
   2886.35   7.223     81
   2884.28   7.218     49
    933.59   2.337     93
    926.39   2.319    320
    919.19   2.300    327
    911.99   2.282    102
    338.99   0.849    393
    331.79   0.831    932
    324.46   0.812    371