3-METHOXY-4-NITROBENZYL ALCOHOL

Mass

MS-NW-8075          
3-methoxy-4-nitrobenzyl alcohol
C8H9NO4             (Mass of molecular ion:    183)

   Source Temperature: 170 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      15.0       5.0
      17.0       1.6
      18.0       7.7
      26.0       1.3
      27.0       8.1
      28.0       7.4
      29.0       9.1
      30.0       7.4
      31.0      11.2
      37.0       2.3
      38.0       6.3
      39.0      28.3
      40.0       6.9
      41.0       9.3
      42.0       1.4
      43.0       3.1
      45.0       2.0
      47.0       1.1
      50.0      12.6
      51.0      26.7
      52.0      12.2
      53.0      24.9
      54.0       5.3
      55.0       8.8
      59.0       4.9
      61.0       2.6
      62.0       8.4
      63.0      20.8
      64.0       7.1
      65.0      39.0
      66.0      35.4
      67.0       9.7
      68.0       2.7
      69.0       2.1
      74.0       5.8
      75.0       6.2
      76.0       9.5
      77.0      68.1
      78.0      26.0
      79.0      43.3
      80.0      59.7
      81.0      14.3
      82.0       8.4
      83.0       1.0
      89.0      39.4
      90.0       7.1
      91.0       9.3
      92.0       7.6
      93.0      14.3
      94.0      25.6
      95.0       5.6
      96.0       5.6
      97.0       9.9
      98.0       1.2
     104.0       2.2
     105.0      40.1
     106.0      15.6
     107.0      12.8
     108.0      39.5
     109.0      12.9
     110.0       3.5
     119.0       6.0
     120.0       2.8
     121.0       8.9
     122.0       6.2
     123.0       2.4
     124.0      19.0
     125.0       2.3
     134.0       1.1
     135.0       5.4
     136.0      28.1
     137.0       5.8
     138.0       1.7
     150.0       1.0
     151.0       1.1
     152.0       3.1
     153.0      16.0
     154.0       4.0
     166.0       3.4
     167.0       2.3
     182.0       1.7
     183.0     100.0
     184.0      12.4
     185.0       1.5

Assign. Shift(ppm) A 7.820 B 7.135 C 6.960 D 4.76 E 3.955 F 2.53

     Hz     ppm     Int.

    704.44   7.866    132
    696.25   7.775    160
    639.19   7.138    125
    638.75   7.133    127
    628.50   7.018     57
    627.81   7.010     91
    627.00   7.001     79
    626.19   6.992     77
    619.50   6.918     74
    618.63   6.908     66
    617.88   6.900     64
    617.19   6.892     40
    426.81   4.766    165
    354.25   3.956   1000