Tiglic acid

Mass

MS-IW-4270          
(E)-2-methyl-2-butenoic acid
C5H8O2              (Mass of molecular ion:    100)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       1.9
      26.0       3.6
      27.0      22.6
      28.0      10.5
      29.0      35.9
      37.0       1.0
      38.0       1.9
      39.0      25.6
      40.0       2.0
      41.0      14.1
      42.0       1.4
      43.0       7.7
      44.0       1.1
      45.0       9.0
      49.0       1.0
      50.0       4.4
      51.0       5.1
      52.0       2.0
      53.0      16.3
      54.0      23.8
      55.0      86.9
      56.0       9.6
      57.0       5.6
      58.0       1.6
      60.0       1.7
      67.0       1.0
      69.0       1.2
      71.0       1.7
      72.0       2.8
      73.0       1.8
      81.0       2.5
      82.0      22.2
      83.0      10.7
      85.0      29.1
      86.0       1.3
      99.0       3.8
     100.0     100.0
     101.0       7.9

Assign. Shift(ppm) A 12. B 7.018 C 1.836 D 1.83

     Hz     ppm     Int.

   2816.00   7.047     20
   2814.90   7.044     25
   2810.32   7.032     39
   2808.86   7.029     75
   2807.94   7.026     66
   2806.48   7.023     37
   2803.55   7.016     39
   2802.08   7.012     72
   2801.17   7.010     65
   2799.52   7.005     22
   2798.42   7.003     22
   2796.22   6.997     23
   2794.94   6.994     28
    736.51   1.843    379
    735.23   1.840    509
    733.95   1.837   1000
    728.09   1.822    182
    726.99   1.820    332
    725.89   1.817    276