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3,5-Bis(trifluoromethyl)benzoyl chloride

Product Name 3,5-Bis(trifluoromethyl)benzoyl chloride

CAS785-56-8

MFC9H3ClF6O

MW276.56

¹³CNMR

Mass

MS-NW-9960          
3,5-bis(trifluoromethyl)benzoyl chloride
C9H3ClF6O           (Mass of molecular ion:    276)

   Source Temperature: 230 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      50.0       1.6
      69.0       3.3
      74.0       3.3
      75.0       6.0
      93.0       1.2
      94.0       1.5
      97.0       1.6
      99.0       1.9
     111.0       2.4
     113.0       1.0
     123.0       1.1
     125.0       2.7
     143.0       7.0
     144.0       6.7
     162.0       1.8
     163.0      12.0
     193.0       2.1
     194.0       5.0
     213.0      54.0
     214.0       4.8
     229.0       1.3
     241.0     100.0
     242.0       9.8
     257.0       9.6
     258.0       1.4
     259.0       3.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₃ Cl F₆ O	0.05 ml : 0.5 ml CDCl₃
3,5-bis(trifluoromethyl)benzoyl chloride

    Assign.     Shift(ppm)

      A             8.586
      B             8.219

     Hz     ppm     Int.

   3432.86   8.590    833
   3432.25   8.589    983
   3431.76   8.587   1000
   3431.15   8.586    999
   3430.66   8.585    972
   3285.52   8.221    452
   3284.79   8.220    498
   3284.18   8.218    437

in CDCl3

liquid film

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