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MassMS-NW-9344 2-acetylfluorene C15H12O (Mass of molecular ion: 208)
Source Temperature: 150 °C Sample Temperature: 80 °C Direct, 75 eV
18.0 3.1 39.0 1.1 43.0 19.8 63.0 3.1 69.5 5.2 75.0 1.3 76.0 3.1 81.0 2.2 81.5 5.8 82.0 7.5 82.5 10.8 83.0 1.7 87.0 1.5 88.0 1.7 89.0 5.4 90.0 4.8 91.0 1.4 96.0 4.5 96.5 5.5 113.0 1.0 115.0 3.2 139.0 4.3 162.0 1.8 163.0 13.9 164.0 13.7 165.0 84.1 166.0 15.7 167.0 1.4 178.0 1.8 179.0 1.1 192.0 1.0 193.0 100.0 194.0 15.5 195.0 1.4 208.0 71.2 209.0 11.9 210.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H12 O 0.066 g : 0.5 ml CDCl3 2-acetylfluorene 
Assign. Shift(ppm)
A 8.057 B 7.929 C 7.766 D 7.734 E 7.516 F 7.365 G 7.337 J 3.838 K 2.593
Hz ppm Int.3221.44 8.061 109 3220.70 8.059 140 3219.85 8.057 142 3219.12 8.055 111 3173.95 7.942 72 3173.10 7.940 64 3172.36 7.938 66 3165.89 7.922 87 3165.16 7.920 77 3164.31 7.918 82 3107.54 7.776 66 3106.20 7.773 88 3101.20 7.760 55 3099.49 7.756 81 3094.48 7.743 144 3086.67 7.724 120 3008.67 7.529 53 3007.93 7.527 62 3007.32 7.525 65 3006.23 7.523 48 3001.10 7.510 77 3000.24 7.508 78 2999.27 7.505 61 2945.19 7.370 73 2944.58 7.368 70 2943.85 7.367 74 2937.62 7.351 142 2935.79 7.346 143 2930.30 7.333 109 2928.96 7.329 91 2922.97 7.314 39 2921.51 7.311 30 1533.81 3.838 287 1036.38 2.594 1000 1033.45 2.586 34
in CDCl3
KBr disc
nujol mull
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